中国药房2018，Vol.29Issue(10)：1340-1343,4.DOI:10.6039/j.issn.1001-0408.2018.10.11
青果氯仿萃取部位的化学成分研究
Study on the Chemical Constituents in the Chloroform Extract of Fructus Canarii
摘要
Abstract
OBJECTIVE:To study the chemical constituents in the chloroform extract of Fructus Canarii. METHODS:The chloroform extract of Fructus Canarii was isolated and purified by MCI,Toyopearl HW-40F,reverse-phase C18,Sephadex LH-20 column. The structure of compounds was analyzed and identified by physicochemical properties and spectral data(mass spectrum, hydrogen spectrum and carbon spectrum). RESULTS:Eight compounds were isolated from chloroform extract of Fructus Canarii, namely Dihydrophaseicacid-3′-O-β-D-glucopyranoside(1),3,4-Dihydroxybenzoic acid(2),3-O-galloylquinic acid(3),Gallic acid (4), Ethyl gallate(5), Scopoletin(6), Dllagic acid-4-O-α-L-rhamnopyranoside(7) and Isocorilagin(8). CONCLUSIONS:Compounds 1,2 and 7 were firstly obtained from Fructus Canarii. The study lays foundation for quality evaluation of Fructus Canarii.关键词
青果/化学成分/二氢红花菜豆酸3'-O-β-D-葡萄糖苷/3,4-二羟基苯甲酸/鞣花酸-4-O-α-L-吡喃鼠李糖苷/结构鉴定/氯仿萃取部位Key words
Fructus Canarii/Chemical constituents/Dihydrophaseicacid-3′-O-β-D-glucopyranoside/3/4-dihydroxybenzoic acid/Ellagic acid-4-O-α-L-rhamnopyranoside/Structural identification/Chloroform extract分类
医药卫生引用本文复制引用
杨洛萍,孟涵,谭穗懿,陈金香,段文军..青果氯仿萃取部位的化学成分研究[J].中国药房,2018,29(10):1340-1343,4.基金项目
国家自然科学基金资助项目(No.81772194、41376162) （No.81772194、41376162）
广东省大学生创新创业训练计划项目(No.粤教高函〔2015〕113号) （No.粤教高函〔2015〕113号）
广州市科技计划项目(No.2014J4100159) （No.2014J4100159）
