江西农业学报2018，Vol.30Issue(6)：92-97,6.DOI:10.19386/j.cnki.jxnyxb.2018.06.20
液相色谱串联质谱法测定动物源性食品中喹乙醇代谢物残留量的不确定度分析
Uncertainty Analysis of Determination of Olaquindox Metabolite Residues in Animal-derived Foodstuff by LC/MS/MS
摘要
Abstract
This article evaluated the uncertainty of determination of olaquindox metabolite residues in animal-derived food-stuff by liquid chromatography and tandem mass spectrometry ( LC/MS/MS) through establishing a mathematical model, and ana-lyzed the uncertainty sources of determination of olaquindox metabolite residues in animal-derived foodstuff. Through calculating the each component of the uncertainty, we obtained that: when the residual quantity of olaquindox metabolites in animal-derived foodstuff was 0.39 μg/kg, its expanded uncertainty was 0.06 μg/kg ( k=2) . The evaluation results showed that measurement re-peatability and recovery were the main sources of the uncertainty.关键词
液相色谱串联质谱法/动物源性食品/喹乙醇代谢物/不确定度分析Key words
LC/MS/MS/Animal-derived foodstuff/Olaquindox metabolites/Uncertainty analysis分类
农业科技引用本文复制引用
罗媛媛,万伟杰,胡丽芳..液相色谱串联质谱法测定动物源性食品中喹乙醇代谢物残留量的不确定度分析[J].江西农业学报,2018,30(6):92-97,6.基金项目
国家畜禽产品质量安全风险评估专项( GJFP2017007) （ GJFP2017007）
农业废弃物再利用的安全评价( JXXTCX2016003-06). （ JXXTCX2016003-06）
