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微波辅助法一步合成荧光碳点用于水中三价铁离子的检测

徐源 陈艳华 丁兰

高等学校化学学报2018,Vol.39Issue(7):1420-1426,7.
高等学校化学学报2018,Vol.39Issue(7):1420-1426,7.DOI:10.7503/cjcu20180031

微波辅助法一步合成荧光碳点用于水中三价铁离子的检测

One-pot Microwave-assisted Synthesis of Passivated Fluorescent Carbon Dots for Fe(Ⅲ)Detection

徐源 1陈艳华 1丁兰1

作者信息

  • 1. 吉林大学化学学院,长春130012
  • 折叠

摘要

Abstract

Carbon dots(CDs)were synthesized through one-pot microwave-assisted synthesis method using citric acid as carbon source,glycerol as solvent and passivation agent.The obtained CDs have uniform size and good dispersion.The proposed synthesis method is rapid,simple and eco-friendly.The CDs were applied to detecting Fe3+in practical water samples based on fluorescence(FL)quenching mechanism with a linear range of 5—50 μmol/L,a detection limit of 2.16 μmol/L and the recoveries of 96.8%—106.0%,which showed good feasibility in detection of Fe3+in practical water samples.

关键词

碳点/微波辅助法/Fe3+检测/荧光猝灭法

Key words

Carbon dots/Microwave-assisted method/Fe3+ detection/Fluorescence quenching method

分类

化学化工

引用本文复制引用

徐源,陈艳华,丁兰..微波辅助法一步合成荧光碳点用于水中三价铁离子的检测[J].高等学校化学学报,2018,39(7):1420-1426,7.

基金项目

吉林省科技厅项目(批准号:20150204070GX)资助.Supported by the Development Program of the Ministry of Science and Technology of Jilin Province,China(No.20150204070GX). (批准号:20150204070GX)

高等学校化学学报

OA北大核心CSCDCSTPCD

0251-0790

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