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小分子羟基硅油为封端剂制备107胶

张大伟 高占臣 吕素芳 蒋剑雄 张飞豹

杭州师范大学学报(自然科学版)2019,Vol.18Issue(1):22-25,4.
杭州师范大学学报(自然科学版)2019,Vol.18Issue(1):22-25,4.DOI:10.3969/j.issn.1674-232X.2019.01.006

小分子羟基硅油为封端剂制备107胶

Synthesis of 107 Adhesive with Small Molecule Hydroxyl Silicone Oil as the Blocking Agent

张大伟 1高占臣 1吕素芳 1蒋剑雄 1张飞豹1

作者信息

  • 1. 杭州师范大学有机硅化学及材料技术教育部重点实验室,浙江 杭州 311121
  • 折叠

摘要

Abstract

107 adhesive was prepared successfully with dimethylcyclotrisiloxane as the raw material, small molecule hydroxyl silicone oil as the blocking agent and potassium hydroxide gel as the catalyst.The structure of the product was characterized by H1-NMR and IR spectrum.The results indicated that taking small molecule hydroxyl silicone oil as the blocking agent could effectively avoid the vaporization problem of water as the blocking agent at high temperature.

关键词

聚合/端羟基聚二甲基硅氧烷/107胶/小分子羟基硅油

Key words

polymerization/hydroxyl terminated polydimethylsiloxanes/107 adhesive/small molecule hydroxyl silicone oil

分类

化学化工

引用本文复制引用

张大伟,高占臣,吕素芳,蒋剑雄,张飞豹..小分子羟基硅油为封端剂制备107胶[J].杭州师范大学学报(自然科学版),2019,18(1):22-25,4.

基金项目

浙江省自然科学基金项目(LY18B040003) (LY18B040003)

高层次留学回国人员(团队)在杭创业创新资助项目 (团队)

氟硅精细化学品与材料制造协同创新中心开放基金项目(FSi2018C003) (FSi2018C003)

杭州师范大学学报(自然科学版)

OACSTPCD

1674-232X

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