特产研究2019，Vol.41Issue(1)：65-67,3.DOI:10.16720/j.cnki.tcyj.2019.01.014
屑止康胶囊质量控制方法研究
Quality Control Method of Xiezhikang Capsule
李忻 1汪旭 2孟庆妍 3朱昆1
作者信息
- 1. 吉林大学中日联谊医院药学部,长春 130021
- 2. 长春市中心医院制剂室,长春 130024
- 3. 吉林省食品药品检验所,长春 130033
- 折叠
摘要
Abstract
The quality control method of Xiezhikang capsule was established.Chromatographic column:Agilent TC-C18 4.6 mm×250 mm, 5 μm);mobile phase:acetonitrile-0.1％ acetic acid solution;gradient elution conditions:0-22 min 14:86, 22 min-27 min 98:2, 27 min-33 min14:86;detection wavelength:230 nm;flow rate:1.0 mL/min;column temperature;25 ℃.The injection volume of paeoniflorin ranged from0.174 0-1.045 1 g.The average recovery was 99.76％, RSD=1.09％ (n=6).The quality standard established in this study is simple, stable and reproducible. It can be used to control the quality of Xiezhikang capsules.关键词
屑止康胶囊/高效液相色谱法/芍药苷/含量测定Key words
Xiezhikang capsule/HPLC/Paeoniflorin/content determination分类
医药卫生引用本文复制引用
李忻,汪旭,孟庆妍,朱昆..屑止康胶囊质量控制方法研究[J].特产研究,2019,41(1):65-67,3.
