云南化工2018,Vol.45Issue(11):75-76,2.DOI:10.3969/j.issn.1004-275X.2018.11.028
原子吸收光谱石墨炉法和火焰法测定卷烟辅料中铅的比较
Contrast Analysis of the Graphite furnace atomic absorption spectrometry and flame method for Plumbum in Cigarette accessories detection
曾彦波 1王春琼 2朱丹1
作者信息
- 1. 红云红河集团会泽卷烟厂, 云南 会泽 654200
- 2. 云南省烟草质量监督检测站, 云南 昆明 650106
- 折叠
摘要
Abstract
(Objective) using respectively atomic absorption spectrometric graphite furnace and flame method to detect unknown aqueous solution, to compare the effects of determination of Plumbum in the same aqueous solution. (Methods) Several samples from the same water solution containing Plumbum were under the suitable oncentration for the standard curve of the graphite furnace and flame method, respectively, and then they were detected and the results were calculated. (Results) The testing result is basically the same, the recovery rate of graphite furnace was 99.89%~102.31% (n=5), and the recovery rate of flame method was 99.93%~102.10% (n=5).Two different samples were measured by using two methods, the relative deviation was in the range of 1.55%~1.71%. (Conclusion) The testing result is basically the same, the method of flame is faster simpler and more Precise, but the graphite furnace method has smaller demand for the sample.关键词
石墨炉法/火焰法/铅Key words
graphite furnace atomic absorption spectrometry/flame atomic absorption spectrophotometry/Plumbum分类
化学化工引用本文复制引用
曾彦波,王春琼,朱丹..原子吸收光谱石墨炉法和火焰法测定卷烟辅料中铅的比较[J].云南化工,2018,45(11):75-76,2.