中国现代中药2019，Vol.21Issue(2)：173-175,193,4.DOI:10.13313/j.issn.1673-4890.20180904011
基于GC-MS技术对甘肃陇南大红袍花椒挥发油柠檬烯 芳樟醇含量的测定
Determination of Limonene and Linalool in Volatile Oil of Dahongpao Zanthoxylum bungeanum in Longnan by GC-MS
摘要
Abstract
Objective:To establish a rapid and sensitive detection method for the determination of limonene and linalool in Zanthoxylum bungeanum, and provide a research method for the quality control of Dahongpao Z.bungeanum in Longnan.Methods:The volatile oil of Dahongpao Z.bungeanum in Longnan was extracted by steam distillation.And it's limonene and linalool were analyzed by gas chromatography-mass.Hexane is used as a thinner.Results:The content of limonene in Dahongpao Z.bungeanum was 0.37％±0.04％, and the content of linalool is 1.07％±0.16％.Conclusion:The GC-MS method established in this paper is sensitive, rapid and accurate, and can be used for the quality control and chemical composition determination of Dahongpao Z.bungeanum in Longnan.关键词
甘肃陇南大红袍花椒/柠檬烯/芳樟醇/气相色谱-质谱法Key words
Dahongpao Zanthoxylum bungeanum in Longnan/limonene/linalool/gas chromatography-mass spectrometry分类
医药卫生引用本文复制引用
司昕蕾,蔡秀荣,曹瑞,边甜甜,辛二旦,牛江涛,张爱霞,李越峰..基于GC-MS技术对甘肃陇南大红袍花椒挥发油柠檬烯 芳樟醇含量的测定[J].中国现代中药,2019,21(2):173-175,193,4.基金项目
国家自然科学基金资助项目 (81460611)；国家教育部科学技术研究重点基金资助项目 (212186)；甘肃省自然科学基金资助项目 (2010:1010RJZA212 （81460611）
2014:145RJZA076)；甘肃省财政厅高校基本科研业务费专项基金资金项目 (2013-2)；兰州市科技局项目 (2014-1-188)；甘肃省中医药管理局科研课题 (GZK-2015-57)；自然科学基金创新基地和人才计划项目 (18JR3RA197)；2018年度甘肃省中药质量与标准研究重点实验室开放基金 (ZYZL18-008)；甘肃中医药大学研究生创新基金 (CX2018-27) （2013-2）
