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SnS2纳米片的制备及其对NO2气体的检测

山巍 傅正钱 张发强 马名生 刘志甫 李永祥

无机材料学报2020,Vol.35Issue(4):497-504,8.
无机材料学报2020,Vol.35Issue(4):497-504,8.DOI:10.15541/jim20190133

SnS2纳米片的制备及其对NO2气体的检测

SnS2 Nanoplates: Synthesis and NO2 Sensing Property

山巍 1傅正钱 2张发强 1马名生 1刘志甫 1李永祥1

作者信息

  • 1. 中国科学院 上海硅酸盐研究所,上海200050
  • 2. 中国科学院大学 材料与光电研究中心,北京100049
  • 折叠

摘要

Abstract

Two-dimensional (2D) metal sulfide materials are ideal for use in gas sensing applications due to their low electronic noise and a large specific surface area, and the research on highly efficient and morphologically controllable methods for preparing two-dimensional metal sulfide materials is necessary. Highly crystalline 2D hexagonal SnS2 nano-plates (NPs) with different morphologies were prepared by high temperature chemical bath method. SnS2 NPs were char-acterized by different techniques, and their gas sensing properties were further investigated. The results show that when the molar ratio of oleic acid (OAc) to oleylamine (OAm) is 1 : 1, the shape of typical SnS2 NPs is a uniform hexagon, with a diameter of about 150 nm and a thickness of 4-6 nm. The gas sensing test shows typical SnS2 NPs are responsive to NO2 gas, and the sensing process is reversible and selective. The optimal operating temperature is 130 ℃, and the re-sponse and recovery time are 98 and 680 s, respectively.

关键词

二氧化氮气体/二维材料/SnS2/高温化学浴法/气敏检测

Key words

NO2 gas/2D materials/SnS2/chemical bath synthesis/gas sensing detection

分类

化学化工

引用本文复制引用

山巍,傅正钱,张发强,马名生,刘志甫,李永祥..SnS2纳米片的制备及其对NO2气体的检测[J].无机材料学报,2020,35(4):497-504,8.

基金项目

National Natural Science Foundation of China (51502325, 61601444) (51502325, 61601444)

无机材料学报

OA北大核心CSCDCSTPCDSCI

1000-324X

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