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低温烧结碳化硅陶瓷分离膜的制备及其油水分离性能

付锦绣 翟凤瑞 李双

硅酸盐学报2022,Vol.50Issue(6):1572-1581,10.
硅酸盐学报2022,Vol.50Issue(6):1572-1581,10.DOI:10.14062/j.issn.0454-5648.20211163

低温烧结碳化硅陶瓷分离膜的制备及其油水分离性能

Low-Temperature Preparation of Silicon Carbide Ceramic Membrane for Oil-in-Water Separation

付锦绣 1翟凤瑞 2李双1

作者信息

  • 1. 山东理工大学资源与环境工程学院,山东 淄博 255049
  • 2. 红河学院,云南 蒙自 661199
  • 折叠

摘要

Abstract

Silicon carbide ceramic membranes can be used in various water and wastewater treatments due to their high hydrophility, and superior chemical and thermal resistances. However, their applications are restricted due to some corresponding problems like high sintering temperature and then the high production cost. In this work, a low-temperature aid (LTA) bonded SiC ceramic symmetric membrane was sintered at 1000 ℃. The results show that LTA bonded SiC particles to form a skeleton of the symmetric membrane. The porosity of the membrane decreases from 42% to 35% and the average pore size decreases from 3.5 μm to 2.1 μm with the increase of LTA content from 10%(mass fraction) to 30%. Based on the results of the separation test on oil-in-water emulsion, the oil rejection and flow flux are 93.3% and 123 L/(m2·h) at the trans-membrane pressure of 0.2 bar, respectively. This study provides a low sintering temperature and energy saving strategy for the preparation of SiC ceramic membrane.

关键词

碳化硅/气孔率/陶瓷膜/油水分离/烧结助剂

Key words

silicon carbide/porosity/membrane/oil-water mixture/sintering aid

分类

通用工业技术

引用本文复制引用

付锦绣,翟凤瑞,李双..低温烧结碳化硅陶瓷分离膜的制备及其油水分离性能[J].硅酸盐学报,2022,50(6):1572-1581,10.

基金项目

山东省自然科学基金(ZR2020MEM027和ZR2020MEM026)资助. (ZR2020MEM027和ZR2020MEM026)

硅酸盐学报

OA北大核心CSCDCSTPCD

0454-5648

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