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CVI处理对浸渍裂解法制备C/C-SiC复合材料弯曲性能的影响

贾林涛 王梦千 郭小凤 朱界 李爱军 彭雨晴

新型炭材料(中英文)2023,Vol.38Issue(6):1127-1134,8.
新型炭材料(中英文)2023,Vol.38Issue(6):1127-1134,8.DOI:10.1016/S1872-5805(23)60732-2

CVI处理对浸渍裂解法制备C/C-SiC复合材料弯曲性能的影响

Effect of chemical vapor infiltration on the flexural properties of C/C-SiC composites prepared by the precursor infiltration pyrolysis method

贾林涛 1王梦千 1郭小凤 1朱界 1李爱军 1彭雨晴1

作者信息

  • 1. 上海大学 材料科学与工程学院 材料研究所,上海 200444
  • 折叠

摘要

Abstract

Carbon/carbon-silicon carbide(C/C-SiC)composites were prepared by impregnation,hot-pressing with curing,carbon-ization at 800 oC and high-temperature heat treatment(800-1600 oC)using a 2D laminated carbon cloth as the reinforcing filler,and furfurone resin mixed with silicon,carbon from furfurone resin and SiC powders as the matrix.The effects of the addition of the three powders as well as subsequent chemical vapor infiltration(CVI)by methane on the density,microstructure and bend strength of the composites were investigated by scanning electron microscopy,density measurements,X-ray diffraction and mechanical testing.Both the SiC powders formed by the reaction at 1600 oC between the added Si and C particles and the added SiC powder,play a role in the reinforcement of the materials.In three-point bending,the composites had a pseudoplastic fracture mode and showed interlam-inar cracking.After 10 h CVI with methane,pyrolytic carbon was formed at the interface between some of the carbon fibers and the resin carbon matrix,which produced maximum increases in the density and flexural strength of the composites of 4.98%and 38.86%,respectively.

关键词

糠酮树脂/C/C-SiC复合材料/无机粉体/化学气相渗透/抗弯强度

Key words

Furfurone resin/C/C-SiC composites/Inorganic powder/CVI/Flexural strength

分类

化学化工

引用本文复制引用

贾林涛,王梦千,郭小凤,朱界,李爱军,彭雨晴..CVI处理对浸渍裂解法制备C/C-SiC复合材料弯曲性能的影响[J].新型炭材料(中英文),2023,38(6):1127-1134,8.

基金项目

National Natural Science Foundation of China(21676163,51602189),Aeronautical Science Founda-tion of China(2016ZFS6001,2017ZFS6001)and The Shanghai Natural Science Fund(No. 18ZR1417700). 国家自然科学基金项目(21676163,51602189) (21676163,51602189)

航空科学基金(2016ZFS6001,2017ZFS6001) (2016ZFS6001,2017ZFS6001)

上海市自然科学基金(18ZR1417700). (18ZR1417700)

新型炭材料(中英文)

OA北大核心CSCDCSTPCD

1007-8827

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