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湿法预处理-电感耦合等离子体原子发射光谱法测定低冰镍的金、银、铂、钯含量

史博洋 刘宇 王皓莹 朱明伟 任晨阳

中国资源综合利用2023,Vol.41Issue(12):41-44,4.
中国资源综合利用2023,Vol.41Issue(12):41-44,4.DOI:10.3969/j.issn.1008-9500.2023.12.012

湿法预处理-电感耦合等离子体原子发射光谱法测定低冰镍的金、银、铂、钯含量

Determination of Gold,Silver,Platinum,and Palladium Content in Low-Nickel Matte by Wet Pretreatment-Inductively Coupled Plasma Atomic Emission Spectroscopy

史博洋 1刘宇 1王皓莹 1朱明伟 1任晨阳1

作者信息

  • 1. 北矿检测技术股份有限公司,北京 102628
  • 折叠

摘要

Abstract

In this experiment,nitric acid and sulfuric acid are used for pretreatment to remove elements such as copper and nickel from low-nickel matte,then the precious metals in low-nickel matte are enriched and impurities are removed by using the fire assay method,subsequently,the contents of gold,silver,platinum,and palladium are determined by using inductively coupled plasma atomic emission spectroscopy(ICP-AES).The experimental results show that this method can achieve a lower detection limit and a wider detection range,and copper has been removed in the pretreatment,reducing the use of lead oxide and achieving the detection of multiple elements,meeting the detection requirements for large sample sizes.

关键词

湿法预处理/ICP-AES/低冰镍/测定////

Key words

wet pretreatment/ICP-AES/low-nickel matte/determination/gold/silver/platinum/palladium

分类

化学化工

引用本文复制引用

史博洋,刘宇,王皓莹,朱明伟,任晨阳..湿法预处理-电感耦合等离子体原子发射光谱法测定低冰镍的金、银、铂、钯含量[J].中国资源综合利用,2023,41(12):41-44,4.

基金项目

十四五国家重点研发计划(2021YFC2903101). (2021YFC2903101)

中国资源综合利用

OACHSSCD

1008-9500

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