中国资源综合利用2023,Vol.41Issue(12):41-44,4.DOI:10.3969/j.issn.1008-9500.2023.12.012
湿法预处理-电感耦合等离子体原子发射光谱法测定低冰镍的金、银、铂、钯含量
Determination of Gold,Silver,Platinum,and Palladium Content in Low-Nickel Matte by Wet Pretreatment-Inductively Coupled Plasma Atomic Emission Spectroscopy
摘要
Abstract
In this experiment,nitric acid and sulfuric acid are used for pretreatment to remove elements such as copper and nickel from low-nickel matte,then the precious metals in low-nickel matte are enriched and impurities are removed by using the fire assay method,subsequently,the contents of gold,silver,platinum,and palladium are determined by using inductively coupled plasma atomic emission spectroscopy(ICP-AES).The experimental results show that this method can achieve a lower detection limit and a wider detection range,and copper has been removed in the pretreatment,reducing the use of lead oxide and achieving the detection of multiple elements,meeting the detection requirements for large sample sizes.关键词
湿法预处理/ICP-AES/低冰镍/测定/金/银/铂/钯Key words
wet pretreatment/ICP-AES/low-nickel matte/determination/gold/silver/platinum/palladium分类
化学化工引用本文复制引用
史博洋,刘宇,王皓莹,朱明伟,任晨阳..湿法预处理-电感耦合等离子体原子发射光谱法测定低冰镍的金、银、铂、钯含量[J].中国资源综合利用,2023,41(12):41-44,4.基金项目
十四五国家重点研发计划(2021YFC2903101). (2021YFC2903101)