中国标准化Issue(2)：183-186,190,5.DOI:10.3969/j.issn.1002-5944.2024.02.032
电感耦合等离子体质谱法在固体废弃物半定量分析中的研究
Study on Semi-quantitative Analysis of Solid Waste by Inductively Coupled Plasma Mass Spectrometry
摘要
Abstract
In order to quickly analyze the types and concentration ranges of metal elements in solid waste,a semi-quantitative analysis method for metal elements in solid waste using inductively coupled plasma mass spectrometry(ICP-MS)by collision/reaction cell was developed.Analysis was conducted on solid waste and reference materials generated in four different typical industries.The experimental results showed that this semi-quantitative analysis method is very suitable for samples with a single and uniform matrix such as reference materials,and has a high accuracy.The relative error of each element was within±10%;The relative deviation of the semi quantitative analysis results of actual samples was within 30%,and the relative deviation of V,Ni,As,Sr,Ba was even controlled within 10%.For solid waste samples with different matrices,this semi-quantitative analysis method has good quantitative ability for sample analysis at concentration levels of μg/L～mg/L.The method is simple,quick and accurate,and can be used as a reliable rapid analysis method for preliminary screening of solid waste,identification of hazard characteristics,water pollution and other environmental emergencies.关键词
电感耦合等离子体质谱法/固体废弃物/半定量分析/突发环境事件Key words
inductively coupled plasma mass spectrometry/solid waste/semi-quantitative analysis/emergent environmental incident引用本文复制引用
连旭,韩凤云,刘中贤,吴恩凯,马宏朕,刘崇书..电感耦合等离子体质谱法在固体废弃物半定量分析中的研究[J].中国标准化,2024,(2):183-186,190,5.基金项目
本文受山东省质检院储备项目"土壤及固体废物样品中重金属半定量分析的方法研究"(项目编号:2019ZJY021)资助. （项目编号:2019ZJY021）
