大学化学2023，Vol.38Issue(12)：61-66,6.DOI:10.3866/PKU.DXHX202304090
星状多席夫碱的设计及多途径合成及表征
Design,Multi-Path Synthesis and Characterization of Stellate Polyschiff Base:A Chemistry Scientific Training Experiment
摘要
Abstract
The Comprehensive Science Training Experiment is a crucial component in the cultivation of top-notch talents in the field of scientific innovation.This article introduces a comprehensive experiment on the synthesis and characterization of a star-shaped polyamine in the organic chemistry science training course.Through this experiment,students can gain an understanding of the cutting-edge research and advancements in polyamine chemistry,apply their theoretical knowledge to design synthetic routes for target products,deepen their understanding of the basic principles and experimental methods of diazotization,Schiff base reaction,and Suzuki coupling reaction,master the techniques of monitoring reactions using thin-layer chromatography and separating products through column chromatography,and learn to characterize and identify compound structures using modern analytical methods such as nuclear magnetic resonance and infrared spectroscopy.This experiment not only cultivates students'rigorous scientific attitude and research innovation consciousness but also trains their practical research skills.Furthermore,through diversified experimental approaches,it fosters students'teamwork abilities,stimulates their enthusiasm,initiative,and creativity,and enhances their problem-analysis-and-solving capabilities.关键词
席夫碱/铃木偶联反应/综合创新实验Key words
Schiff base/Suzuki coupling reaction/Comprehensive innovation experiment分类
社会科学引用本文复制引用
李一鸣,王本花,魏保生,宋相志,罗一鸣,喻桂朋..星状多席夫碱的设计及多途径合成及表征[J].大学化学,2023,38(12):61-66,6.基金项目
湖南省教育厅重点项目(2022jy077) （2022jy077）
中南大学教育教学改革项目(2023JGB081) （2023JGB081）
