均匀化处理对激光选区熔化GH3536和GH4169合金组织和显微硬度的影响OA北大核心CSTPCD
Effect of homogenizing treatment on microstructure and microhardness of GH3536 and GH4169 alloy by selective laser melting
GH3536和GH4169镍基高温合金常用来制造航空发动机等热端部件.采用激光选区熔化(selective laser melting,SLM)最优工艺参数制备GH3536和GH4169合金试样,研究不同均匀化温度和保温时间对两种合金组织演变、平均晶粒尺寸和性能的影响,利用OM、SEM、EDS等方法表征其缺陷特征和微观组织,利用维氏硬度仪测试合金的显微硬度.结果表明:成形态GH3536合金中存在更多缺陷,包括气孔、裂纹和未熔合;成形态GH4169合金中只存在气孔.均匀化处理使合金熔池消失,使晶粒长大成为等轴晶.GH3536合金晶界和晶内有M23C6 析出,GH4169合金晶界和晶内有NbC析出,随着均匀化温度升高,析出物明显减少.GH3536合金的平均晶粒尺寸从1130℃,1 h的 48.5 μm增大到 1250℃,4 h的 100.9 μm,增大了 106.8%;GH4169的平均晶粒尺寸从 1080℃,1 h时的 57 μm增大到 1200℃,4 h时的 87.4 μm,增加了 53.3%.GH3536合金经过均匀化处理后显微硬度下降明显,由原来 262HV下降到 180~190HV;与之相反,GH4169合金经过均匀化处理后硬度提高,显微硬度均保持在430~450HV之间,明显高于成形态试样的313HV.
GH3536 and GH4169 nickel-based superalloys are widely used in aerospace engines and other hot-end components.In this paper,GH3536 and GH4169 alloy samples were fabricated by optimizing the process parameters using selective laser melting(SLM),the defect characteristics and microstructure of two alloys,as well as the effects of different homogenization temperatures and holding times on microstructure evolution,average grain size,and properties of two alloys were studied.The defect characteristics and microstructure were investigated by OM,SEM,and EDS,et al.The Vickers hardness meter was used to test the alloy's microhardness.The results indicate that the as-built GH3536 alloy exhibits more defects,including pores,cracks,and lack of fusion,while only pores are present in as-built GH4169 alloy.The melt pool of alloy is eliminated by homogenization treatment,and the grains grow into equiaxed grains.M23C6 are found to distribute within grain boundaries and grain interiors of GH3536 alloy,while NbC are found to distribute within grain boundaries and grain interiors of GH4169 alloy,and the amount of precipitates is significantly reduced with the increase of homogenization temperature.The average grain size of GH3536 alloy is increased by 106.8%from 48.5 μm at 1130℃/1 h to 100.9 μm at 1250℃/4 h.The grain size of GH4169 alloy is increased by 53.3%from 57 μm at 1080℃/1 h to 87.4 μm at 1200℃/4 h.The homogenization treatment of GH3536 alloy and GH4169 alloy results in a significant decrease in microhardness of the former,from 262HV to 180-190HV,while the latter shows a significant increase,from 313HV to 430-450HV.
耿硕;张冬云;李健民;仪登豪;池煜璟;黄帅;张学军
北京工业大学 物理与光电工程学院,北京 100124||北京市数字化医疗 3D打印工程技术研究中心,北京 100124中国航发北京航空材料研究院,北京 100095
激光选区熔化GH3536GH4169微观组织均匀化热处理平均晶粒尺寸显微硬度
selective laser meltingGH3536GH4169microstructurehomogenizing treatmentaverage grain sizemicrohardness
《航空材料学报》 2024 (001)
72-83 / 12
中国航空发动机集团产学研合作项目(HFZL2021CXY020)
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