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三苯基铋与三对甲苯基铋的合成

陈静 何仕艳 蒲娅玲 谢竹 唐薇 黎凤娇

合成材料老化与应用2024,Vol.53Issue(1):70-72,3.
合成材料老化与应用2024,Vol.53Issue(1):70-72,3.

三苯基铋与三对甲苯基铋的合成

Synthesis of Triphenylbismuth and Tri-p-tolylbismuth

陈静 1何仕艳 1蒲娅玲 1谢竹 1唐薇 1黎凤娇1

作者信息

  • 1. 四川文理学院化学化工学院,四川达州 635000
  • 折叠

摘要

Abstract

Triarylbismuth compounds have been used in organic synthesis and catalysis because of their relatively stable properties.The Grignard reagent were prepared from aryl bromide and magnesium in tetrahydrofuran solution,and then reacted with bismuth trichloride to synthesize triarylbismuth compounds.The effects of reaction temperature and reaction time on reaction yield have been discussed.Through the optimization of reaction conditions,the yields of triphenylbismuth and tri-p-tolylbismuth reached 52%and 63%,respectively.

关键词

三苯基铋/三对甲苯基铋/合成条件

Key words

triphenylbismuth/tri-p-tolylbismuth/synthesis condition

分类

化学化工

引用本文复制引用

陈静,何仕艳,蒲娅玲,谢竹,唐薇,黎凤娇..三苯基铋与三对甲苯基铋的合成[J].合成材料老化与应用,2024,53(1):70-72,3.

基金项目

四川文理学院博士专项科研基金项目(2019BS015Z) (2019BS015Z)

省级大学生创新创业训练计划项目(S202210644133). (S202210644133)

合成材料老化与应用

OACSTPCD

1671-5381

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