中药材2023，Vol.46Issue(8)：1937-1941,5.DOI:10.13863/j.issn1001-4454.2023.08.016
黑桑枝化学成分研究
Chemical Constituents from Twigs of Morus nigra
摘要
Abstract
Objective:To study the chemical constituents from the twigs of Morus nigra.Methods:The ethyl acetate fraction of Mo-rus nigra twigs was isolated and purified by HP20 macroporous resin column choromatography,normal-phase silica gel,Sephadex LH-20 and semi-preparative liquid chromatography,and the structures were identified by modern spectral methods(UV,IR,MS,NMR).Re-sults:Nine compounds were isolated from the twigs of Morus nigra and identified as 2',4',2"-trihydroxychalcone-4"-O-β-D-glucoside(1),quercetin(2),2,4-dihydroxybenzaldehyde(3),taxifolin(4),3-O-methylquercetin(5),3-O-methylquercetin-7-O-β-D-glucoside(6),morin(7),quercetin-3'-O-β-D-glucoside(8),quercetin-4'-O-β-D-glucoside(9),respectively.Conclusion:Among them,compound 1 is a new chalcone glucoside,compounds 1,5,6 and 9 are isolated from Morus nigra for the first time.关键词
黑桑枝/化学成分/黄酮类Key words
Twigs of Morus nigra L./Chemical constituents/Flavonoids分类
医药卫生引用本文复制引用
高薇,魏沣,唐辉,庞克坚,杨新洲..黑桑枝化学成分研究[J].中药材,2023,46(8):1937-1941,5.基金项目
国家自然科学基金项目(82160796) （82160796）
