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半枫荷叶正丁醇部位的化学成分研究

裘硕 陈月圆 孙佳祺 李典鹏 卢凤来 颜小捷

中药材2023,Vol.46Issue(8):1946-1950,5.
中药材2023,Vol.46Issue(8):1946-1950,5.DOI:10.13863/j.issn1001-4454.2023.08.018

半枫荷叶正丁醇部位的化学成分研究

Chemical Constituents of n-Butanol Extract from the Leaves of Semiliquidambar cathayensis

裘硕 1陈月圆 1孙佳祺 2李典鹏 1卢凤来 1颜小捷1

作者信息

  • 1. 广西壮族自治区中国科学院广西植物研究所/广西植物功能物质与资源持续利用重点实验室,广西 桂林 541006
  • 2. 广西壮族自治区中国科学院广西植物研究所/广西植物功能物质与资源持续利用重点实验室,广西 桂林 541006||桂林医学院,广西 桂林 541006
  • 折叠

摘要

Abstract

Objective:To study the chemical constituents of n-butanol extract from the leaves of Semiliquidambar cathayensis.Methods:The compounds from the n-butyl alcohol faction of acetone extract of the leaves of Semiliquidambar cathayensis were isolated and purified by column chromatography and semi-preparative HPLC,the structures were identified by means of physicochemical proper-ties and 1 D-NMR spectra data.Results:Thirteen compounds were isolated from the n-butanol faction of acetone extract of the leaves of Semiliquidambar cathayensis and identified as neochlorogenic acid(1),4-hydroxy-2-methoxyphenol-1-O-β-D-(6'-O-galloyl)-glucoside(2),4-hydroxy-3-methoxyphenol-1-O-β-D-(6'-O-galloyl)-glucoside(3),rutin(4),hyperoside(5),isoquercitrin(6),kaempferol-3-O-β-D-rutinoside(7),astragalin(8),myricetin-3-O-(6"-galloyl)-β-D-glucopyranoside(9),kaempferol-3-O-α-L-rhamnoside(10),di-hydromyricetin(11),astragalin-6"-O-gallate(12),myricetin-3-O-(6"-galloyl)-β-D-galactopyranoside(13),respectively.Conclusion:All compounds are isolated from Semiliquidambar cathayensis for the first time.

关键词

半枫荷/化学成分/黄酮

Key words

Semiliquidambar cathayensis Chang/Chemical constituents/Flavonoids

分类

医药卫生

引用本文复制引用

裘硕,陈月圆,孙佳祺,李典鹏,卢凤来,颜小捷..半枫荷叶正丁醇部位的化学成分研究[J].中药材,2023,46(8):1946-1950,5.

基金项目

广西自然科学基金项目(2020GXNSFBA297055) (2020GXNSFBA297055)

广东省重点领域研发计划项目(2020B1111110003) (2020B1111110003)

广西科学院基本科研业务费(2019YJJ1003) (2019YJJ1003)

桂林市创新平台和人才计划(20210102-3) (20210102-3)

中药材

OA北大核心CSTPCD

1001-4454

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