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气质联用法测定湘西香醋中7种挥发性成分

饶青青

吉首大学学报(自然科学版)2024,Vol.45Issue(1):61-65,5.
吉首大学学报(自然科学版)2024,Vol.45Issue(1):61-65,5.DOI:10.13438/j.cnki.jdzk.2024.01.011

气质联用法测定湘西香醋中7种挥发性成分

Determination of Seven Volatile Components in Xiangxi Aromatic Vinegar by GC-MS

饶青青1

作者信息

  • 1. 湘西土家族苗族自治州食品药品检验所,湖南吉首 416000
  • 折叠

摘要

Abstract

The Xiangxi aromatic vinegar were pretreatmented by SDE,and the content of ethyl acetate,ethanol,ethyl lactate,2,3-butanedione,3-hydroxyl-2-butanone,furfural and 2,3-butanediol was determi-nated by GC-MS.HP-INNOWAX capillary gas chromatographic column and GC-MS-HS were used.The sample inlet temperature was 220 ℃,the split ratio was 40∶1,the fourth stage rod temperature was 230℃,the ion source temperature was 230 ℃,and SIM mode was used.The results showed that linear rela-tionship was between 0.991 and 0.999,and the method repeatability was less than 10%,which indicates that this method can be used for the determination of volatile components in Xiangxi aromatic vinegar.

关键词

湘西香醋/气质联用法/挥发性成分/蒸馏萃取法

Key words

Xiangxi aromatic vinegar/GC-MS/volatile components/SDE

分类

信息技术与安全科学

引用本文复制引用

饶青青..气质联用法测定湘西香醋中7种挥发性成分[J].吉首大学学报(自然科学版),2024,45(1):61-65,5.

吉首大学学报(自然科学版)

1007-2985

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