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民族药毛大丁草化学成分研究

高奇 杨柳 李齐激 文雯 周浪 杨小生 杨娟

中药材2023,Vol.46Issue(7):1688-1692,5.
中药材2023,Vol.46Issue(7):1688-1692,5.DOI:10.13863/j.issn1001-4454.2023.07.017

民族药毛大丁草化学成分研究

Chemical Constituents of Ethnodrug Gerbera piloselloides

高奇 1杨柳 2李齐激 1文雯 2周浪 1杨小生 1杨娟1

作者信息

  • 1. 贵州医科大学省部共建药用植物功效与利用国家重点实验室 550014||贵州省中国科学院天然产物化学重点实验室,贵州 贵阳 550014
  • 2. 贵州省中国科学院天然产物化学重点实验室,贵州 贵阳 550014
  • 折叠

摘要

Abstract

Objective:To study the chemical constituents of Gerbera piloselloides.Methods:The compounds from the ethanol extract of Gerbera piloselloides were isolated and purified by silica gel column chromatography,preparation liquid phase and recrystallization methods.The structures of the compounds were identified by NMR,MS spectrometry.Results:Twenty compounds were isolated from the ethanol extract of Gerbera piloselloides and identified as 3,5-bis(3,3-dimethylallyl)-4-hydroxyacetophen-one(1),2-[(2S∗)-6-acetyl-2,3-dihydro-5-ydroxybenzofuran-2-yl]prop-2-enyl-3-methylbutanoate(2),adian-5-en-3α-ol(3),aspergillus triazolate A(4),methyl lino-leate(5),sesamin(6),5-acetyl-2-(2-hydroxyisopropyl)-7-(3,3-dimethylallyl)-2,3-dihydrobenzofuran(7),shearene A(8),4-hydroxyacetophenone(9),4-hydroxybenzaldehyde(10),kaempferol(11),1H-indole-3-carboxaldehyde(12),ursolic aldehyde(13),ethyl caffeate(14),2,5-dihydroxyacetophenone(15),luteolin(16),caffeic acid(17),ferulic acid(18),arbutin(19),hydroquinone(20),respectively.Conclusion:Among them,compounds 1 to 14 are isolated from Gerbera piloselloides for the first time.

关键词

毛大丁草/化学成分/分离鉴定

Key words

Gerbera piloselloides(L.)Cass./Chemical constituents/Isolation and identification

分类

医药卫生

引用本文复制引用

高奇,杨柳,李齐激,文雯,周浪,杨小生,杨娟..民族药毛大丁草化学成分研究[J].中药材,2023,46(7):1688-1692,5.

基金项目

贵州省科技创新能力建设专项(黔科合服企[2020]4013) (黔科合服企[2020]4013)

贵州省天然产物高效利用工程研究中心(黔财建[2019]303) (黔财建[2019]303)

贵州食药用生物资源可持续利用特色重点实验室(黔教合KY字[2020]018) (黔教合KY字[2020]018)

中药材

OA北大核心CSTPCD

1001-4454

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