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含钴萃余液中和除杂及钴回收试验研究

付晨晓 姚现召

中国资源综合利用2024,Vol.42Issue(3):1-4,4.
中国资源综合利用2024,Vol.42Issue(3):1-4,4.DOI:10.3969/j.issn.1008-9500.2024.03.001

含钴萃余液中和除杂及钴回收试验研究

Experimental Study on Neutralization,Impurity Removal,and Cobalt Recovery of Cobalt Containing Raffinate

付晨晓 1姚现召1

作者信息

  • 1. 华刚矿业股份有限公司,北京 100039
  • 折叠

摘要

Abstract

The experiment uses the copper raffinate from a certain copper cobalt ore recovery process as raw material,and adopts the neutralization impurity removal-cobalt precipitation process to recover cobalt hydroxide products.The results show that from the optimal conditions for neutralization and impurity removal,the reaction temperature is 80℃,the endpoint pH is 5.0~5.5,the air flow rate is 400 L/min,the stirring speed is 2 200 r/min,and the reaction time is 4 h.Under optimal conditions,the precipitation rates of Al,Fe,and Mn are 98.66%,98.81%,and 8.53%,respectively,while the precipitation rate of Co is only 0.21%.Subsequently,MgO cobalt precipitation is carried out on the impurity removal solution,and the Co precipitation rate exceeds 99%,during the cobalt precipitation process,maintaining an inert atmosphere has a significant inhibitory effect on Mn precipitation.

关键词

钴回收/萃余液/除杂/氧化镁

Key words

cobalt recovery/raffinate/impurity removal/magnesium oxide

分类

矿业与冶金

引用本文复制引用

付晨晓,姚现召..含钴萃余液中和除杂及钴回收试验研究[J].中国资源综合利用,2024,42(3):1-4,4.

中国资源综合利用

OACHSSCD

1008-9500

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