炸药造型颗粒随机堆积体系物理参量无损表征OA北大核心CSTPCD
Non-destructive Characterization of Physical Parameters in Random Packing Systems of Explosive Molding Granules
炸药造型颗粒作为高聚物粘结炸药(Polymer-bonded explosive,PBX)构件成型的中间体,表征其体系物理参量对掌握不同造型颗粒对PBX构件性能的影响具有重要意义.利用X射线层析成像(XCT)和图像处理技术无损表征了9种造型颗粒样品随机堆积体系(包含粒径、体积分数、孔隙率、球形度以及本征密度)的物理参量.9种造型颗粒堆积体系平均粒径最大为1.04 mm,体积分数最高可达68.7%,孔隙率最低为1.04%,平均球形度最高为0.93,密度最大为1.44 g·cm-3.结果表明,造型颗粒配方中粘结剂种类、炸药晶体成分、炸药晶体配比以及造粒工艺对颗粒堆积体系物理参量有重要影响,且颗粒堆积体系物理参量之间存在相关性.体系粒径分布越分散,颗粒平均表面积越大;体系平均粒径越大、平均球形度越低,颗粒平均孔隙率就越高;平均粒径较大的颗粒堆积体系体积分数较高,当体系平均球形度较大时颗粒堆积的体积分数与球形度无关.研究为掌握造型颗粒堆积体系的物理参量以及颗粒结构与材料性能关系提供了基础.
The molding granule is an intermediate for polymer-bonded explosive(PBX)components.Characterization of the physical parameters of granular system is of great significance to understanding the influence of different granule structure on the performance of PBX components.X-ray computed micro-tomography(XCT)and CT image processing were used to non-destructively characterize physical parameters(including granule diameter,volume fraction,porosity,sphericity and intrin-sic density)of the granular random packing systems.The average granule diameter of granular systems is up to 1.04 mm,the vol-ume fraction is up to 68.7%,the lowest porosity is 1.04%,the highest average sphericity is 0.93,and the highest density is 1.44 g·cm-3.Results show that the type of binder,composition and ratio of explosive crystals,and granulation process have a pronounced influence on the physical parameters of granular packing systems.Moreover,there is a correlation between physical parameters of granular systems.The more dispersed diameter distribution of granular system leads to the larger the average sur-face area of granules.The larger average granule diameter and lower average sphericity of granular system result in the higher po-rosity of the granules.The volume fraction of granular systems with larger average granule diameter is higher,and the volume fraction of the granule accumulation is independent of the sphericity when the average sphericity is large.This research provides fundamental insights into understanding the physical parameters and their associations with material properties in molding granu-lar packing systems.
岳弘历;张催;张伟斌
中国工程物理研究院化工材料研究所,四川 绵阳 621999
武器工业
炸药造型颗粒随机堆积体系体积分数孔隙率X射线层析成像
explosive molding granulerandom packing systemvolume fractionporosityX-ray tomography
《含能材料》 2024 (004)
345-352 / 8
国家自然科学基金青年基金(12105267) National Natural Science Foundation of China(No.12105267)
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