广东药科大学学报2024，Vol.40Issue(2)：16-22,7.DOI:10.16809/j.cnki.2096-3653.2024012307
苍耳子标准汤剂的质量标准研究
Study on quality standard of Xanthii Fructs standard decoction
摘要
Abstract
Objective To establish the quality standard of Xanthii Fructs standard decoction.Methods According to the traditional decocting method,12 batches of Xanthii Fructs standard decoction were prepared,the range of the paste yield was determined,and the characteristic spectra of Xanthii Fructs standard decoction were established by HPLC.TLC was used for qualitative identification using chlorogenic acid and Xanthii Fructs as reference material.Results The extraction rate of 12 batches of Xanthii Fructs standard decoction ranged from 6.0%to 9.9%,with an average of 8.1%.10 common peaks were marked and 8 components were identified,namely,neochlorogenic acid(peak 2),chlorogenic acid(peak 3),cryptochlorogenic acid(peak 4),caffeic acid(peak 5),1,3-O-dicaffeoyl quinic acid(peak 6),isochlorogenic acid B(peak 7),3,5-O-dicaffeoyl quinic acid(peak 8),4,5-O-dicaffeoyl quinic acid(peak 10).TLC spots were clear,the separation degree was good,and the translational value was appropriate.Conclusion The established quality standard is reasonable and reliable,which can provide reference for the quality control of Xanthii Fructs formula granule.关键词
苍耳子/标准汤剂/特征图谱/薄层鉴别Key words
Xanthii Fructs/standard decoction/Characteristic map/TLC分类
医药卫生引用本文复制引用
魏家保,唐双燕,詹智洪,谢嘉慧,赵伟志,黄凯伟,张辉,谭沛..苍耳子标准汤剂的质量标准研究[J].广东药科大学学报,2024,40(2):16-22,7.基金项目
深圳市科技计划项目(JSGG20191129093418578) （JSGG20191129093418578）
