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响应面试验优化柿子皮多糖铬的制备工艺研究

苗旭忠 李秀芬 高艳艳 张雪 张禧庆 乔鲁芹

山东科学2024,Vol.37Issue(2):127-134,8.
山东科学2024,Vol.37Issue(2):127-134,8.DOI:10.3976/j.issn.1002-4026.20230088

响应面试验优化柿子皮多糖铬的制备工艺研究

Optimization of preparation of persimmon peel polysaccharide chromium using response surface methodology

苗旭忠 1李秀芬 2高艳艳 3张雪 3张禧庆 4乔鲁芹1

作者信息

  • 1. 山东农业大学 植物保护学院山东省林业有害生物防控工程技术研究中心,山东泰安 271018
  • 2. 泰山风景名胜区管理委员会,山东 泰安 271018
  • 3. 临沂市沂南县检测中心,山东临沂 276300
  • 4. 山东杰诺检测服务有限公司,山东烟台 265200
  • 折叠

摘要

Abstract

In this study,the hot water extraction method was utilized to extract polysaccharides from persimmon peel,and the persimmon peel polysaccharides were combined with trivalent chromium ions to prepare persimmon peel polysaccharide chromium.Considering the adsorption rate of chromium as the index,the adsorption process of persimmon peel polysaccharide chromium was optimized using single factor and response surface methodology.The results showed that the optimal preparation process of persimmon peel polysaccharide chromium consisted of the following steps,such as the mass ratio of persimmon peel polysaccharides to chromium chloride was set at 6.7:1;the reaction time was 150 min;the temperature was set at 82 ℃;and the pH of the adsorption liquid was fixed at 5.Under these conditions,the maximum adsorption rate reached 92.81%.Therefore,this study has shown that persimmon peel polysaccharides can efficiently bind trivalent chromium ions,which can further provide technical support for the development of green pollution-free heavy-adsorption chromium adsorbents or animal nutritional supplements.

关键词

柿子皮/多糖/铬吸附/响应面试验

Key words

persimmon peel/polysaccharide/chromium adsorption rate/response surface methodology

分类

轻工业

引用本文复制引用

苗旭忠,李秀芬,高艳艳,张雪,张禧庆,乔鲁芹..响应面试验优化柿子皮多糖铬的制备工艺研究[J].山东科学,2024,37(2):127-134,8.

山东科学

OACSTPCD

1002-4026

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