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X射线荧光光谱法测定滑石粉中组分含量

李国燕

中国非金属矿工业导刊Issue(2):73-75,83,4.
中国非金属矿工业导刊Issue(2):73-75,83,4.

X射线荧光光谱法测定滑石粉中组分含量

Determination of Components in Talcum Powder by X-ray Fluorescence Spectrometry

李国燕1

作者信息

  • 1. 桂林桂广滑石开发有限公司,广西 桂林 541199
  • 折叠

摘要

Abstract

A quantitative analysis method for the determination of SiO2,MgO,Fe2O3,Al2O3 and CaO in talcum powder by X-ray fluorescence spectrometry with boric acid powder tablet was introduced.According to the content range of primary and secondary components in talc,the calibration curve is drawn by using the commercially available talc standard sample and the production product which has been determined by chemical analysis method as the standard sample.Eliminate the influence of absorption and enhancement effect by empirical coefficient matrix correction method.Boric acid is used as the mixing agent,and the mass ratio of talcum powder(200~400mesh)to boric acid is 5:1,which is fully mixed by vibration grinding,and then the sample with smooth surface is pressed by a press machine.The precision test and comparison test show that the error between the standard sample and the standard value determined by this analysis method is completely within the allowable error range of the national standard.The content of components in talcum powder is determined,and the detection value is consistent with the detection value by chemical method,which realizes simple,rapid and accurate determination.

关键词

粉末压片/X射线荧光光谱法/滑石粉

Key words

pressed powder pellet/X-ray fluorescence spectrometry/talcum powder

分类

天文与地球科学

引用本文复制引用

李国燕..X射线荧光光谱法测定滑石粉中组分含量[J].中国非金属矿工业导刊,2024,(2):73-75,83,4.

基金项目

广西重点研发计划项目"龙胜滑石矿综合利用及精深加工技术研发与应用示范"(编号:桂科AB21076013). (编号:桂科AB21076013)

中国非金属矿工业导刊

OACSTPCD

1007-9386

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