电泳共沉积法制备金刚石/Al2O3/玻璃复合涂层的工艺OACSTPCD
Preparation of Diamond/Al2O3/Glass Composite Coating by Electrophoretic Co-Deposition Method
以304不锈钢为基体,采用电泳共沉积法制备复合涂层,并通过烧结方式实现涂层在基体的固化.研究电泳共沉积过程中不同悬浮液组成、沉积电压、沉积时间和Al3+质量分数等因素对涂层性能的影响,对涂层进行微观结构表征和力学性能测试,并使用该工艺制备抛光盘,用于蓝宝石的抛光.结果表明:当沉积电压为50 V,沉积时间为6 min,添加质量分数为0.10%的Al3+时,可获得光滑、均匀的金刚石/Al2O3/玻璃复合涂层;复合涂层经450 ℃烧结3 h后,表面致密均匀,硬度达521 HV,复合涂层的耐磨性、与基体的结合强度均良好;使用抛光盘对蓝宝石进行抛光,可将表面粗糙度降低90.2%.
Diamond/A12O3/glass composite coating was prepared by electrophoretic co-deposition method on 304 stainless steel substrate,and curing of the coating on the substrate was realized through sintering method.The influence of suspension compositions,deposition voltage,deposition time and mass fraction of Al3+on the coating properties during the electrophoretic co-deposition process was investigated.Microstructure character-ization and mechanical property testing of the prepared coating were carried out,and polishing discs were pre-pared using this process for polishing sapphire substrate.The results showed that smooth and uniform dia-mond/Al2O3/glass composite coating was obtained when the deposition voltage was 50 V,the deposition time was 6 min and Al3+with mass fraction of 0.10%was added.The composite coating had a dense and uniform surface with a hardness of 521 HV after being sintered at 450 ℃ for 3 h,it also exhibited excellent abrasion re-sistance and bond strength with the substrate.The surface roughness of sapphire substrate was reduced by 90.2%after polishing using the prepared polishing discs.
薛志萍;陆静;毛现艳;黄身桂;郭桦
华侨大学制造工程研究院,福建厦门 361021||华侨大学脆性材料产品智能制造技术国家地方联合工程研究中心,福建厦门 361021||华侨大学生物质低碳转化福建省高校重点实验室,福建厦门 361021华侨大学制造工程研究院,福建厦门 361021||华侨大学脆性材料产品智能制造技术国家地方联合工程研究中心,福建厦门 361021
金刚石电泳共沉积复合涂层烧结抛光盘
diamondelectrophoretic co-depositioncomposite coatingsinteringpolishing disc
《华侨大学学报(自然科学版)》 2024 (003)
303-313 / 11
国家自然科学基金资助项目(51975222,51835004);福建省自然科学基金资助项目(2021J06027);华侨大学先进碳转化技术研究院开放基金(2023年度)
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