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ICP-OES有机直接进样法测定食品添加剂中铁、钙、铝、铅、锌、砷

荣沙沙 杜建侠 李红 肖清燕 卢会珍

云南化工2024,Vol.51Issue(4):101-103,3.
云南化工2024,Vol.51Issue(4):101-103,3.DOI:10.3969/j.issn.1004-275X.2024.04.24

ICP-OES有机直接进样法测定食品添加剂中铁、钙、铝、铅、锌、砷

Determination of Iron,Calcium,Aluminum,Lead,Zinc and Arsenic in Food Additives by Directly Introduction under Method of Organic Phase Using ICP-OES

荣沙沙 1杜建侠 1李红 1肖清燕 1卢会珍1

作者信息

  • 1. 湖北三峡实验室,湖北 宜昌 443000
  • 折叠

摘要

Abstract

Inductively Coupled Plasma Optical Emission Spectrometer(ICP-OES)was proposed to determine of 6 elements including iron,calci-um,aluminum,lead,zinc and arsenic in food additives by directly introduction under method of organic phase.With ethanol solution as a diluent,the samples are directly analyzed after being diluted according to a specific ratio,the results showed that good linearity in the concentration range of 0.05-5.00 mg/L and the correlation coefficient was over 0.9999,the limits of detection(LODs)of all the elements were in the range from 0.0001-0.0016 mg/L,the average recoveries were 91.4%-108.4%,and the relative standard deviations(RSD)were 0.53%-3.65%.This method is simple to operate,highly accurate,safe and fast.It can be used for detecting impurity elements in compound food additives.

关键词

ICP-OES/有机进样法/食品添加剂/杂质元素

Key words

ICP-OES/Method of Organic Phase Sampling/Food Additives/Impurity Elements

分类

化学化工

引用本文复制引用

荣沙沙,杜建侠,李红,肖清燕,卢会珍..ICP-OES有机直接进样法测定食品添加剂中铁、钙、铝、铅、锌、砷[J].云南化工,2024,51(4):101-103,3.

云南化工

1004-275X

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