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大颗粒掺铝四氧化三钴的制备条件优化

夏勇 祝婷

电源技术2024,Vol.48Issue(5):869-873,5.
电源技术2024,Vol.48Issue(5):869-873,5.DOI:10.3969/j.issn.1002-087X.2024.05.014

大颗粒掺铝四氧化三钴的制备条件优化

Optimization of preparation conditions for large particles doped alu-minium cobalt tetroxide

夏勇 1祝婷2

作者信息

  • 1. 湖南中伟新能源科技有限公司,湖南长沙 410600
  • 2. 湖南中联重科应急装备有限公司,湖南长沙 410000
  • 折叠

摘要

Abstract

Large particles of aluminum-doped cobalt tetroxide were prepared by liquid phase precipitation-thermal decomposition.The effects of cobalt liquid flow,reaction temperature and reac-tion pH on impurity S content,solid density and supernatant Co content of large particles of aluminum-doped cobalt carbonate during liquid phase precipitation were investigated.At the same time,the influences of preheating temperature and feeding amount on the vibration density and cracking of large particles doped with aluminum cobalt tetroxide were investigated.The results show that the optimal conditions for precipitation of large particles of aluminum-doped cobalt carbonate are the feed flow of cobalt liquid 2.5 L/h,reaction temperature 45℃and pH 7.4.The optimal condi-tions for sintering are 30 m3/h and 15 kg/h cobalt carbonate feed rate.

关键词

掺铝四氧化三钴/碳酸钴/液相沉淀/球形颗粒

Key words

aluminum-doped cobalt tetroxide/cobalt carbonate/liquid phase precipitation/spherical particle

分类

信息技术与安全科学

引用本文复制引用

夏勇,祝婷..大颗粒掺铝四氧化三钴的制备条件优化[J].电源技术,2024,48(5):869-873,5.

电源技术

OA北大核心CSTPCD

1002-087X

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