世界有色金属Issue(6):60-64,5.
电感耦合等离子体原子发射光谱法测定镍合金中的铬含量
Determination of Chromium Content in Nickel Alloy by Inductively Coupled Plasma Atomic Emission Spectroscopy
摘要
Abstract
The method for determination of chromium in nickel alloy in international standard ISO 7530-1:2015 using a nitrous oxide-acetylene flame atomic absorption spectrometry has been rarely used.In this paper,the experimental work on the determination of chromium by inductively coupled plasma atomic emission spectrometry is reported.Through sample dissolution test,sample weighing test,matrix interference test and internal standard selection test,the analytical conditions were optimized,and the analytical method for the determination of chromium in nickel alloy by inductively coupled plasma emission spectrometry was established.The method is accurate and reliable,which meets the requirements of the determination of chromium in nickel alloy.The method is recommended as a national standard.关键词
标准/镍合金/铬含量测定/电感耦合等离子体原子发射光谱法Key words
standard/nickel alloy/determination of chromium content/inductively coupled plasma atomic emission spectrometry分类
矿业与冶金引用本文复制引用
黄基宁,吴兹舜,陈子彦,韦莉,黄肇敏..电感耦合等离子体原子发射光谱法测定镍合金中的铬含量[J].世界有色金属,2024,(6):60-64,5.基金项目
本项目获得了广西科技基地和人才专项资助,项目号:桂科AD20159089 ()
项目并列入国家标准化管理委员会2022年项目计划:《镍合金化学分析方法第8部分:钴、铬、铜、铁和锰含量的测定火焰原子吸收光谱法》(计划编号:20220744-T-610). (计划编号:20220744-T-610)