壳聚糖―肉桂精油微胶囊的制备、表征及其抑菌活性评价OA
Preparation,Characterization and Antibacterial Activity of Chitosan-Cinnamon Essential Oil Microcapsules
为应对肉桂精油刺激性气味大、水溶性差、易挥发等限制其自身于食品行业应用的性质,采用壳聚糖作为壁材对其进行微胶囊化处理.以包埋率为指标,通过单因素实验及响应面法优化制备工艺,对壳聚糖-肉桂精油微胶囊进行性质表征并评价其对食源性致病菌的抑菌活性.结果表明,壳聚糖与肉桂精油质量比为 1∶1.04,壳聚糖与乳化剂吐温-80 质量比为1∶1.14,壳聚糖与交联剂三聚磷酸钠质量比为 2.24∶1 时,肉桂精油微胶囊包埋率和包埋得率分别为 14.74%±1.18%和8.14%±0.23%.该微胶囊具有较优异的热稳定性及缓释效果,属于非菲克扩散效应,且展现出较优异的抑菌活性.
To enhance the cinnamon essential oil limited properties of unpleasure flavor,limited solubility and volatility in food industry,chitosan was used as the wall material for microencapsulation treatment.Optimization of preparation process of chitosan-cinnamon essential oil microcapsules was evaluated by single factor experiments and response surface methodology based on the encapsulation efficiency.The characterization and evaluation of antibacterial activity against food-borne pathogenic bacteria were investigated as well.The optimum technological conditions of chitosan-CEO microcapsules were as followed:chitosan-CEO mass ratio 1∶1.04,chitosan-tween-80 mass ratio 1∶1.14 and chitosan-sodium tripolyphosphate mass ratio 2.24∶1.Correspondingly,the encapsulation efficiency and loading capability was 14.74%±1.18%and 8.14%±0.23%,respectively.It showed relatively excellent thermal stability and cumulative releasing effect,which was related to non-fickian diffusion effect.Besides,the chitosan-cinnamon essential oil microcapsules also showed relatively superior antibacterial activity.
黄兆翔;王永玲;谭少健;高佳敏;杜磊
中科检测技术服务(广州)股份有限公司,广东 广州 510650
轻工业
肉桂精油微胶囊制备工艺性质表征抑菌活性
cinnamon essential oilmicroencapsulationpreparation technologycharacterizationantibacterial activity
《纤维素科学与技术》 2024 (002)
14-22 / 9
评论