大学化学2024，Vol.39Issue(6)：303-311,9.DOI:10.3866/PKU.DXHX202312006
基于Raman光谱的3,5-二氨基-1,2,4-三唑(DAT)合成反应在线监测与反应机理探究——推荐一个仪器分析综合实验
Online Monitoring and Mechanistic Analysis of 3,5-diamino-1,2,4-triazole (DAT) Synthesis via Raman Spectroscopy:A Recommendation for a Comprehensive Instrumental Analysis Experiment
摘要
Abstract
This paper presents a comprehensive instrumental analysis experiment featuring online monitoring of 3,5-diamino-1,2,4-triazole (DAT) synthesis via Raman spectroscopy and the exploration of the reaction mechanism. Highlighting a synthesis that integrates instrumental analysis with scientific research,the experiment encompasses DAT synthesis,online reaction monitoring,and mechanism analysis through Raman spectroscopy. By employing chemometric techniques for the analysis of Raman spectral data,the study offers profound insights into the synthesis process,deepening the understanding of the reaction mechanism. This experiment reinforces students' chemical knowledge,improves their practical laboratory skills,ignites their passion for scientific investigation,and develops their capabilities for research and inquiry.关键词
拉曼光谱/在线监测/合成反应机理/综合实验Key words
Raman spectroscopy/Online monitoring/Synthesis reaction mechanism/Comprehensive experiment分类
社会科学引用本文复制引用
张天龙,张容玲,汤宏胜,李延,李华..基于Raman光谱的3,5-二氨基-1,2,4-三唑(DAT)合成反应在线监测与反应机理探究——推荐一个仪器分析综合实验[J].大学化学,2024,39(6):303-311,9.基金项目
教育部高等学校化学类专业教学指导委员会教学研究与实践项目(H20210602,H20210603) （H20210602,H20210603）
教育部基础学科拔尖学生培养计划2.0研究课题(20222159) （20222159）
