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挤压刺梨牛肉干中维生素C损失预测模型OACSTPCD

Prediction model for vitamin C loss in extruded prickly Rosa roxburghii Tratt beef jerky

中文摘要英文摘要

为了探索挤压刺梨牛肉干中维生素C(VC)的损失规律,解决挤压过程中营养物质损失的"黑箱"问题,本文使用双螺杆挤压机生产刺梨牛肉干,采用高效液相色谱法测定物料挤压前后的VC含量,得到挤压前后的VC损失率.以碳粉为示踪剂,测定物料在挤压机内的停留时间,将平均停留时间(MRT,记作tm)视为不同条件下物料在挤压机内的反应时间,对不同挤压条件下VC损失率进行动力学分析,通过多项式回归分析得到不同机筒温度、螺杆转速条件下的VC损失率预测模型.结果表明,挤压过程中VC损失率与机筒温度、螺杆转速均呈显著负相关,与刺梨添加量影响不显著.动力学分析表明,不同挤压条件下VC的损失速率常数(k)为 0.003 54~0.006 05 s-1,通过多项式回归分析得到k、tm对不同机筒温度、螺杆转速条件下的预测模型,相关系数R2分别为0.756 4和0.971 2,模型拟合度较高,可实现对挤压过程中营养物质损失规律的合理预测.

The purpose of this paper is to explore the principle of vitamin C loss in extruded Rosa roxburghii Tratt beef jerky and investigate the"black box"problem of nutrient loss during the extrusion process.By using Rosa roxburghii Tratt beef jerky produced with a twin-screw extruder,we measured the vitamin C contents before and after extrusion by HPLC,then calculated the vitamin C loss rate during this process.Moreover,we collected the residence time of the material in the extruder by using toner as the tracer,and the mean value was considered to be the reaction time.Based on the kinetic analysis of VC loss rates under different extrusion conditions with various barrel temperatures and screw speeds,a VC loss rate prediction model was established using polynomial regression analysis method.As a result,the VC loss rates were negatively correlated with barrel temperatures and screw speeds,despite the amounts of Rosa roxburghii Tratt.In addition,dynamic analysis could generate the vitamin C loss rate constant,which was between 0.003 54 and 0.006 05 s-1 under different extrusion conditions.Further polynomial regression analysis provided the prediction models of k and tm for different barrel temperatures and screw rotation speeds,with the R2 values as 0.756 4 and 0.971 2,respectively.The well-fitted models could reasonably predict the nutrient loss in the extrusion process.

马秀兰;李静鹏;苏婕妤;张广涛;张汝平;王明科;赖虹睿;邓力

贵州大学 酿酒与食品工程学院,贵州 贵阳 550000西安安聚徳纳米科技有限公司,陕西 西安 710000贵州五福坊食品(集团)股份有限公司,贵州 贵阳 550000

轻工业

双螺杆挤压刺梨牛肉干维生素C损失率预测模型营养物质损失

twin-screw extrusionRosa roxburghii Tratt beef jerkyvitamin C loss rateprediction modelnutrient loss

《生物加工过程》 2024 (004)

432-439 / 8

国家自然科学基金(32260642);贵州省科技计划(黔科合支撑[2022]重点002号、黔科合基础-ZK[2022]一般066、黔科合支撑[2021]一般177);贵州省教育厅项目(S202210657097);贵州大学引进人才科研项目(贵大人基合字(2020)号)

10.3969/j.issn.1672-3678.2024.04.010

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