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关节植入物表面多孔涂层形貌结构和耐磨性能的检测研究

李帆 王常斌 高娜 梁金奎 方元 张露文 杨婧 张博

中国医疗设备2024,Vol.39Issue(8):38-43,6.
中国医疗设备2024,Vol.39Issue(8):38-43,6.DOI:10.3969/j.issn.1674-1633.2024.08.006

关节植入物表面多孔涂层形貌结构和耐磨性能的检测研究

Study on Morphological Structure and Wear Resistance of Porous Coatings on the Surface of Joint Implants

李帆 1王常斌 1高娜 1梁金奎 1方元 1张露文 1杨婧 1张博1

作者信息

  • 1. 山东省医疗器械和药品包装检验研究院,山东济南 250101||国家药品监督管理局生物材料器械安全性评价重点实验室,山东济南 250101||山东省医疗器械生物学评价重点实验室,山东济南 250101
  • 折叠

摘要

Abstract

Objective To analyze and explore the morphological structure,and wear resistance of porous coatings with different processes on the surface of joint implants.Methods Three types of plasma sprayed titanium coating samples,one type of titanium bead sintered coating sample,and one type of 3D printed porous structure sample were selected.The porous structure of the surface coating of the samples were analyzed according to YY/T 0988.14-2016,and the porosity and pore intercept of the porous structure were measured on the longitudinal section of coating under metallographic microscope.And the wear resistance of the samples were tested according to ASTM F1978-22.The surface morphology of the coating before and after wear were observed under a scanning electron microscope,and the wear behavior and wear mechanism of coatings with different processes and pore structures were analyzed.Results The porosity of several coatings ranged from 30%to 60%,with a pore intercept between 100 and 510 μm,in compliance with FDA regulations,the pore connectivity of titanium bead sintered coatings and 3D printed porous coatings were better than that of plasma sprayed coatings.The wear process of plasma sprayed coatings was characterized by particle detachment accompanied by abrasive wear,while the wear process of titanium bead sintered coatings and 3D printed porous samples was mainly characterized by abrasive wear.Conclusion The difference in wear resistance is significantly related to coating process,porosity,and structural form.

关键词

等离子喷涂/3D打印/涂层形貌/耐磨性能

Key words

plasma sprayed/3D printed/coating morphology/wear resistance

分类

预防医学

引用本文复制引用

李帆,王常斌,高娜,梁金奎,方元,张露文,杨婧,张博..关节植入物表面多孔涂层形貌结构和耐磨性能的检测研究[J].中国医疗设备,2024,39(8):38-43,6.

基金项目

山东省医疗器械和药品包装检验研究院课题(NB202311). (NB202311)

中国医疗设备

OACSTPCD

1674-1633

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