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电感耦合等离子体原子发射光谱法测定锌冶炼物料中铊含量

郑丽霞 杨月 于亮

世界有色金属Issue(14):157-159,3.
世界有色金属Issue(14):157-159,3.

电感耦合等离子体原子发射光谱法测定锌冶炼物料中铊含量

Determination of thallium content in zinc smelting materials by Inductively coupled plasma atomic emission spectrometry

郑丽霞 1杨月 1于亮1

作者信息

  • 1. 株洲冶炼集团股份有限公司,湖南 株洲 412000
  • 折叠

摘要

Abstract

Aqua regia was used to dissolve the sample,Tl190.856nm was selected as the analysis line,and the inductively coupled plasma atomic emission spectrometry(ICP-AES)was established,the thallium mass concentration was in the range of 0.0020%~0.050%,and the spectral line intensity showed a good linear relationship,the correlation coefficient r was 0.99999,and the detection limit of thallium was 0.0076μg/mL.The test method is applied to the determination of thallium in zinc smelting materials,and the relative standard deviation RSD of the results is less than 4.62%,and the recovery rate is 90%~103%,which can be used to efficiently and simply determine the determination of thallium content in zinc smelting system.

关键词

ICP-AES/回收率/

Key words

ICP-AES/Recovery/Thallium

分类

矿业与冶金

引用本文复制引用

郑丽霞,杨月,于亮..电感耦合等离子体原子发射光谱法测定锌冶炼物料中铊含量[J].世界有色金属,2024,(14):157-159,3.

世界有色金属

1002-5065

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