世界有色金属Issue(14):157-159,3.
电感耦合等离子体原子发射光谱法测定锌冶炼物料中铊含量
Determination of thallium content in zinc smelting materials by Inductively coupled plasma atomic emission spectrometry
郑丽霞 1杨月 1于亮1
作者信息
- 1. 株洲冶炼集团股份有限公司,湖南 株洲 412000
- 折叠
摘要
Abstract
Aqua regia was used to dissolve the sample,Tl190.856nm was selected as the analysis line,and the inductively coupled plasma atomic emission spectrometry(ICP-AES)was established,the thallium mass concentration was in the range of 0.0020%~0.050%,and the spectral line intensity showed a good linear relationship,the correlation coefficient r was 0.99999,and the detection limit of thallium was 0.0076μg/mL.The test method is applied to the determination of thallium in zinc smelting materials,and the relative standard deviation RSD of the results is less than 4.62%,and the recovery rate is 90%~103%,which can be used to efficiently and simply determine the determination of thallium content in zinc smelting system.关键词
ICP-AES/回收率/铊Key words
ICP-AES/Recovery/Thallium分类
矿业与冶金引用本文复制引用
郑丽霞,杨月,于亮..电感耦合等离子体原子发射光谱法测定锌冶炼物料中铊含量[J].世界有色金属,2024,(14):157-159,3.