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气相分子吸收光谱法测定水中氨氮的方法验证

李荧荧

中国标准化Issue(20):173-177,5.
中国标准化Issue(20):173-177,5.DOI:10.3969/j.issn.1002-5944.2024.20.032

气相分子吸收光谱法测定水中氨氮的方法验证

Validation of the Method for Determining Ammonia Nitrogen in Water by Gas Phase Molecular Absorption Spectrometry

李荧荧1

作者信息

  • 1. 辽宁省锦州水文局
  • 折叠

摘要

Abstract

In this paper,HJ 195-2023,Water quality—Determination of ammonia nitrogen by gas-phase molecular absorption spectrometry,is used for the study of validating the method for the determination of ammonia nitrogen in water by gas molecular absorption spectrometry.The verification content mainly includes linearity calibration curve,method detection limit,lower limit of determination,precision,accuracy and other aspects.The results show that the correlation coefficient of the standard curve is r>0.999,the method detection limit is 0.01 mg/L,the lower limit of determination is 0.02 mg/L,the results of certified reference materials are all within the qualified range,and the add standard recovery is 97.0%~105.8%.The validation results of all performance indicators meet the requirements of the standard,which means the laboratory has the ability to determine ammonia nitrogen in water by gas molecular absorption spectrometry.

关键词

氨氮/气相分子吸收光谱/方法验证

Key words

ammonia nitrogen/gas phase molecular absorption spectrometry/method validation

引用本文复制引用

李荧荧..气相分子吸收光谱法测定水中氨氮的方法验证[J].中国标准化,2024,(20):173-177,5.

中国标准化

OACHSSCD

1002-5944

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