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氮气流量对氮化钛涂层微观结构与性能的影响

李健智 李文元 潘旭 罗侃 丁泽良

包装学报2024,Vol.16Issue(5):18-27,51,11.
包装学报2024,Vol.16Issue(5):18-27,51,11.DOI:10.3969/j.issn.1674-7100.2024.05.003

氮气流量对氮化钛涂层微观结构与性能的影响

Influence of Nitrogen Flow Rate on Micro structure and Properties of Titanium Nitride Coatings

李健智 1李文元 1潘旭 1罗侃 1丁泽良1

作者信息

  • 1. 湖南工业大学机械工程学院 湖南 株洲 412007
  • 折叠

摘要

Abstract

Titanium nitride coatings were prepared on Ti6A14V titanium alloy via DC reactive sputtering technology at different nitrogen flow rates.The coating was characterized by scanning electron microscope(SEM),X-ray diffractometer(XRD),X-ray photoelectron spectroscopy(XPS),scratch tester,and electrochemical workstation to investigate the influence of nitrogen flow rate on the coating's microstructure and properties.Results indicate that at 0.3 mL/min nitrogen flow rate,the coating exhibits an amorphous structure,while at 0.5~3.5 mL/min,there is a titanium nitrogen oxide crystal phase.As the nitrogen flow rate increases,the N element content in the coating decreases,the O element content increases,the coating thickness decreases,and the density,interface bonding,and corrosion resistance are enhanced.

关键词

Ti6Al4V/直流反应溅射/氮化钛涂层/结合力/耐蚀性

Key words

Ti6Al4V/DC reactive sputtering/titanium nitride coating/adhesion/corrosion resistance

分类

矿业与冶金

引用本文复制引用

李健智,李文元,潘旭,罗侃,丁泽良..氮气流量对氮化钛涂层微观结构与性能的影响[J].包装学报,2024,16(5):18-27,51,11.

基金项目

湖南省自然科学基金资助项目(2023JJ50163) (2023JJ50163)

包装学报

1674-7100

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