岩矿测试2025，Vol.44Issue(1)：115-126,12.DOI:10.15898/j.ykcs.202401290011
北宋定窑茶叶末釉的微观结构与矿物形态学研究
Microstructure Characterization and Mineral Morphology of Tea-Dust Glaze Made in the Ding Kiln of the Northern Song Dynasty
摘要
Abstract
The tea-dust glaze ancient porcelain is one of the earliest crystalline glazes,which is rarely studied deeply because of its rarity.In this study,the mineral crystals in tea-dust glaze made in the Ding Kiln of the Northern Song Dynasty were analyzed by optical microscope(OM),laser ablation-inductively coupled plasma-mass spectrometry(LA-ICP-MS),scanning electron microscopy coupled with an X-ray energy dispersive spectrometer(SEM-EDS),laser confocal Raman spectrometer(LRS),and high-resolution time of flight-secondary ion mass spectrometry(ToF-SIMS).The results show that the main crystal phase in the glaze is the same as that of the Longquanwu Kiln in the Liao and Jin Dynasty,which is anorthite and augite.The overall performance of the glaze is that the sauce-black glaze matrix is rich in iron(Fe2O3 mean 9.73%)and the mineral crystal is rich in iron(Fe2O3 mean 11.33%).In addition to α-Fe2O3 crystals,Fe3O4 crystals and other recrystallized minerals after melting,the glaze also has pleonaste,residual kaolinite and other unmelted minerals from raw glaze materials.The residual kaolinite shows that the firing temperature of the samples in this study was most likely below 1200℃.The BRIEF REPORT is available for this paper at http://www.ykcs.ac.cn/en/article/doi/10.15898/j.ykcs.202401290011.关键词
茶叶末瓷/矿物/元素成像/ToF-SIMS/LA-ICP-MSKey words
tea-dust glaze/minerals/element imaging/ToF-SIMS/LA-ICP-MS分类
化学引用本文复制引用
徐建业,王富芳,梁汉东,李展平..北宋定窑茶叶末釉的微观结构与矿物形态学研究[J].岩矿测试,2025,44(1):115-126,12.基金项目
国家自然科学基金项目(41371449,41772157) （41371449,41772157）
中央高校基本科研业务费资助项目"太行山东缘煤系地层出露与古窑址分布关系研究"(2022YJSMT01) （2022YJSMT01）
