大连工业大学学报2024，Vol.43Issue(6)：449-453,5.DOI:10.19670/j.cnki.dlgydxxb.2024.0611
铯钨青铜粉体的制备及其近红外屏蔽/隔热性能
Preparation of cesium tungsten bronze powder and its near-infrared shielding/thermal insulation properties
摘要
Abstract
Cesium tungsten bronze powder and its thin film samples were prepared by solid-state reaction and electrospinning-solid-state reaction methods.The crystalline phase composition,micromorphology and near-infrared shielding properties of cesium tungsten bronze powder and thin films were studied by X ray diffraction(XRD),scanning electron microscopy(SEM),transmission electron microscopy(TEM)and ultraviolet-visible-near-infrared(UV-Vis-NIR)spectrophotometer.Besides,the thermal insulation properties of the thin film were tested in a homemade thermal insulation box.The results showed that the particle size of the cesium tungsten bronze powder prepared by the electrospinning-solid-state method(namely samples were calcined directly at 600 ℃ in a tube furnace after spinning)was smaller,which was due to the presence of PVP which restricted the growth of the particles.The prepared powder and film exhibited better NIR shielding performance under the condition of ensuring visible light transmittance of 67.1％,and the near-infrared shielding efficiency was up to 99.99％.关键词
铯钨青铜/固相反应法/静电纺丝/近红外屏蔽Key words
cesium tungsten bronze/solid-state reaction/electrospinning/near-infrared shielding分类
建筑与水利引用本文复制引用
田紫薇,刘敬肖,史非,李艺,王美玉..铯钨青铜粉体的制备及其近红外屏蔽/隔热性能[J].大连工业大学学报,2024,43(6):449-453,5.基金项目
辽宁省教育厅高校基本科研项目(LJKMZ20220887) （LJKMZ20220887）
大连市科技创新基金计划项目(2018J12SN066). （2018J12SN066）
