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气相色谱法测定水果中15种有机磷类农药残留的基质效应

罗贵文 黄告 林思思 陈廷春 刘宏梅 张汉莉

安徽农业科学2024,Vol.52Issue(23):188-191,204,5.
安徽农业科学2024,Vol.52Issue(23):188-191,204,5.DOI:10.3969/j.issn.0517-6611.2024.23.041

气相色谱法测定水果中15种有机磷类农药残留的基质效应

Matrix Effects of 15 Organophosphorus Pesticide Residues in Fruits Determined by Gas Chromatography

罗贵文 1黄告 1林思思 1陈廷春 1刘宏梅 2张汉莉1

作者信息

  • 1. 百色市农产品质量安全检测中心,广西百色 533000
  • 2. 百色市农牧渔技术推广中心,广西百色 533000
  • 折叠

摘要

Abstract

Using 12 blank fruit matrices as solvents,15 organic phosphorus pesticides were prepared into mixed standard solutions of 0.05,0.10,0.20,0.40 and 0.80 mg/L,and compared with acetone solvent.The matrix effect of organic phosphorus pesticide residues in different fruit matrices was determined by gas chromatography.The results showed that 15 organic phosphorus pesticides exhibited varying degrees of matrix effects in 12 fruit substrates,with most pesticides exhibiting matrix enhancement effects,and there was no necessary correlation between pesticides and concentrations.Therefore,when conducting the detection of organic phosphorus pesticide residues in fruits,it is recommended to use a matrix instead of acetone as the solvent for standard preparation,which can greatly reduce the interference of the matrix on the detection results and improve the accuracy of the detection results.

关键词

基质效应/有机磷农药/气相色谱仪/水果

Key words

Matrix effect/Organic phosphorus pesticides/Gas chromatograph/Fruit

分类

轻工纺织

引用本文复制引用

罗贵文,黄告,林思思,陈廷春,刘宏梅,张汉莉..气相色谱法测定水果中15种有机磷类农药残留的基质效应[J].安徽农业科学,2024,52(23):188-191,204,5.

安徽农业科学

0517-6611

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