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电感耦合等离子体发射光谱法测定地质样品中K2O、Na2O、CaO、MgO、Al2O3、Fe2O3、TiO2

闵欣 卢业友 罗文莎

化工矿产地质2024,Vol.46Issue(4):357-362,6.
化工矿产地质2024,Vol.46Issue(4):357-362,6.

电感耦合等离子体发射光谱法测定地质样品中K2O、Na2O、CaO、MgO、Al2O3、Fe2O3、TiO2

Determination of K2O,Na2O,CaO,MgO,Al2O3,Fe2O3 and TiO2 in geological samples by ICP-AES

闵欣 1卢业友 1罗文莎1

作者信息

  • 1. 贵州省有色金属和核工业地质勘查局物化探总队,贵州 都匀 558000
  • 折叠

摘要

Abstract

In this paper,a method for the determination of K2O,Na2O,CaO,MgO,Al2O3,Fe2O3 and TiO2 in geological samples by inductively coupled plasma atomic emission spectrometry(ICP-AES)is established.The main working parameters of the instrument and the analysis of spectral lines,dissolved acid and other melting conditions are studied.The detection limit of each component of the method,the linear range of the working curve,the accuracy and precision of the results are discussed.The results shows that the precision of the method is between 0.57%and 3.09%,and the accuracy is between 0.04%and 2.72%.It meets the detection requirements of"Chemical Composition Analysis of Rock Mineral Samples in Geological Survey Samples".The method is simple,time-consuming,and can simultaneously determine a variety of elements with high precision and good accuracy.It can meet the requirements of batch quantity analysis of K2O,Na2O,CaO,MgO,Al2O3,Fe2O3,and TiO2 of geological samples in laboratory.

关键词

电感耦合等离子体发射光谱法/地质样品/线性范围/精密度/准确度/快速测定

Key words

ICP-AES/Geological samples/linear range/precision/accuracy/rapid determination

分类

化学化工

引用本文复制引用

闵欣,卢业友,罗文莎..电感耦合等离子体发射光谱法测定地质样品中K2O、Na2O、CaO、MgO、Al2O3、Fe2O3、TiO2[J].化工矿产地质,2024,46(4):357-362,6.

基金项目

黔南州地质勘查基金 黔南州罗甸县逢亭镇冶金用石英岩矿产地质勘查(编号:JHC2020J-010FW) (编号:JHC2020J-010FW)

化工矿产地质

1006-5296

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