中国农业科技导报2024,Vol.26Issue(12):122-128,7.DOI:10.13304/j.nykjdb.2023.0247
紫外-可见光谱库在农药杀菌剂隐性排查中的应用
Application of UV-visible Spectral Library in Recessive Screening of Pesticide Fungicides
陈颖 1刘小锋 1陈一萍 1廖丽萍 1傅洪涛1
作者信息
- 1. 湖南化工研究院有限公司,国家农药创制工程技术研究中心,长沙 410014||湖南化肥农药质量监督检验授权站,长沙 410014
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摘要
Abstract
To establish the ultraviolet-visible(UV-VIS)spectral library to quickly and accurately retrieve the hidden components added in the pesticide fungicide,with acetonitrile and water as the mobile phase,the UV-VIS spectrograms of 98 conventional bactericide standards were separated and extracted by gradient elution using a high-performance liquid chromatograph,and the UV-VIS spectrograms of the standard substances were used to establish the UV-VIS spectrogram library.The target compound was matched according to the spectral similarity and the retention time of the standard sample,so as to retrieve the hidden components added in the pesticide preparation.2 bactericides were used to verify the accuracy of the spectral library retrieval,and the results showed that the accuracy of the spectral library retrieval reached 100%.This method had the advantages of high accuracy,easy operation and low cost.关键词
高效液相色谱仪/杀菌剂/紫外-可见光谱库/农药Key words
high-performance liquid chromatography/bactericide/ultraviolet-visible spectrum library/pesticide分类
农业科技引用本文复制引用
陈颖,刘小锋,陈一萍,廖丽萍,傅洪涛..紫外-可见光谱库在农药杀菌剂隐性排查中的应用[J].中国农业科技导报,2024,26(12):122-128,7.