山东医药2024，Vol.64Issue(36)：45-50,6.DOI:10.3969/j.issn.1002-266X.2024.36.009
山慈菇的乙酸乙酯、石油醚、氯仿萃取物挥发性成分鉴定
Identification of volatile ingredients in ethyl acetate,petroleum ether and chloroform extracts of Cremastra appendiculata
摘要
Abstract
Objective To identify the volatile ingredients in ethyl acetate,petroleum ether and chloroform extracts of Cremastra appendiculata.Methods Three kilograms of Cremastra appendiculata were processed into powder and ex-tracted with ethyl acetate,petroleum ether and chloroform,respectively.The volatile ingredients in ethyl acetate extract,petroleum ether extract and chloroform extract were analyzed and identified by gas chromatography-mass spectrometry(GC-MS).Results Fifty-one ingredients were identified from the ethyl acetate extract of Cremastra appendiculata,with the highest content of catechol,followed by 4-hydroxybenzaldehyde,2-ethyl-3-methylpyrazine,Phenol,4-(ethoxymethyl)-,cinnamic acid,m-hydroxybenzoic acid,etc.Thirty-five ingredients were identified from the petroleum ether extract of Cremastra appendiculata,including cinnamic acid,butyl palmitate,methyl heptadecanoate,oleic acid,linoleic acid,etc.Twenty-eight ingredients were identified from the chloroform extract of Cremastra appendiculata,including Phenol,4-(eth-oxymethyl)-,2,6-dimethoxyphenol,2-ethyl-3-methylpyrazine,cinnamic acid,etc.Conclusion Cinnamic acid was found in the volatile ingredients of ethyl acetate,petroleum ether and chloroform extracts of Cremastra appendiculata.Anti-cancer ingredients such as vanillic acid,m-hydroxybenzoic acid and 4-hydroxybenzaldehyde were found in the ethyl acetate extract of Cremastra appendiculata.Catechol,2-ethyl-3-methylpyrazine,Phenol,3-methylcyclopentane-1,2-dione,meth-ylcyclopentenolone,butyl palmitate,methyl heptadecanoate,oleic acid,linoleic acid,2,6-dimethoxyphenol,2-ethyl-3-methylpyrazine and other ingredients were found in different extracts of Cremastra appendiculata for the first time.关键词
山慈菇/乙酸乙酯萃取物/石油醚萃取物/氯仿萃取物/气相色谱—质谱联用法/挥发性成分Key words
Cremastra appendiculata/ethyl acetate extract/petroleum ether extract/chloroform extract/GS-MS/volatile ingredients分类
医药卫生引用本文复制引用
初雨萌,李迪佳,李雅静,姚芳,张子英,高瑞霞..山慈菇的乙酸乙酯、石油醚、氯仿萃取物挥发性成分鉴定[J].山东医药,2024,64(36):45-50,6.基金项目
内蒙古自治区自然科学基金(2024FX33,2023MS08055) （2024FX33,2023MS08055）
内蒙古自治区公立医院高水平临床专科发展科技项目(2023SGGZ106). （2023SGGZ106）
