福建冶金2025，Vol.54Issue(1)：42-45,4.
基于外源硅预处理的重量法测定碳化硅中SiC检测方法的优化研究与应用
Optimization Research and Application of Gravimetric Determination of SiC in Silicon Carbide Based on External Silicon Pretreatment
连小安 1周扬杰1
作者信息
- 1. 福建省冶金工业设计院有限公司,福建 福州 350011
- 折叠
摘要
Abstract
To further optimize the detection of SiC content in silicon carbide,a mixed acid was used to pretreat the exogenous silicon,and then the silicon dioxide content was directly measured by weight method to convert it into SiC content.The method studied the influencing factors such as sample pretreatment method,dosage of perchloric acid,dehydration frequency,and filtrate recovery.According to the experimental method,the SiC content in silicon carbide samples was determined.The relative deviation of the test results was between-0.26%and 0.13%,and the relative standard deviation was between 0.09%and 0.39%.The test results were reliable,accurate,and had good repeatability and reproducibility.关键词
碳化硅/外源硅/重量法/换算Key words
silicon carbide/perchlorate/weight method/silicon dioxide引用本文复制引用
连小安,周扬杰..基于外源硅预处理的重量法测定碳化硅中SiC检测方法的优化研究与应用[J].福建冶金,2025,54(1):42-45,4.
