岩矿测试2024，Vol.43Issue(6)：892-900,9.DOI:10.15898/j.ykcs.202410230223
双极端对比检测法定量分析高纯石英砂气液包裹体含量
Quantitative Detection of Gas-Liquid Inclusions in High-Purity Quartz Sand by Double Extreme Case Analysis
摘要
Abstract
High-purity quartz sand serves as a critical material in various strategic emerging industries,such as semiconductors and photovoltaics.The quality of quartz sand is crucial for the application of products like single crystal silicon crucibles and quartz tubes.Besides impurity elements,gas-liquid inclusions are a significant factor affecting quartz quality.However,current detection methods for gas-liquid inclusions are mainly qualitative,lacking efficient and precise quantitative analysis techniques.The double extreme case analysis(DECA)method is innovatively proposed here to quantitatively assess the content of gas-liquid inclusions.The process involves quartz sand slices treated with reagent and put under a microscope for observation and photographing,obtaining at least 300 images of quartz particles where the quartz appears transparent and the inclusions appear black.By statistically analyzing the images,the ratio of transparent(T)to non-transparent(NT)particles is calculated to evaluate quartz quality.The crucible study of different quartz sands using DECA shows that quartz sand with a high T ratio and low NT ratio produces crucibles of excellent transparency,while quartz sand with a low T ratio and high NT ratio results in poor transparency.This method effectively addresses the challenge of quantitative gas-liquid inclusion detection and provides a reliable basis for evaluating high-purity quartz sand quality.关键词
高纯石英/气液包裹体/定量/双极端对比检测法/石英坩埚Key words
high purity quartz/gas-liquid inclusions/quantification/double extreme case detection method/quartz crucible分类
矿业与冶金引用本文复制引用
樊婷,任子杰,张乾坤,何宇豪,宋昱晗,刘志,向璐..双极端对比检测法定量分析高纯石英砂气液包裹体含量[J].岩矿测试,2024,43(6):892-900,9.基金项目
国家科技重大专项项目(2024ZD0605400) （2024ZD0605400）
