安徽农业科学2025，Vol.53Issue(3)：171-176,6.DOI:10.3969/j.issn.0517-6611.2025.03.036
基于HS-GC-IMS技术评价卷烟的质量稳定性
Evaluation of Quality Stability of Cigarettes Based on HS-GC-IMS Technique
摘要
Abstract
[Objective]Headspace-gas chromatography-ion mobility spectrometry(HS-GC-IMS)was used to analyse the volatile components of cigarette products,and explore its application in the evaluation of cigarette quality stability.[Method]The HS-GC-IMS technique was used to determine the volatile components in different batches of five cigarette samples,analyse the differences of volatile components in different samples based on fingerprinting,and develop the index levels of volatile components contained in different cigarette reference samples,com-pare and analyse the detection results of different cigarette samples,and evaluate the similarity of volatile components of cigarette samples by using the angle-of-concentration cosine method,and combine with the mean-pole-difference(Xbar-R)control chart to evaluate the quality sta-bility of different cigarette samples.[Result]A total of 86 volatile components were detected in different cigarette samples,and the finger-prints showed that there were obvious similarities between different batches of each cigarette sample,and the volatile components among five cigarette samples had their own characteristic peak areas,showing large differences;the angle cosine values between the samples and the refer-ence samples were further calculated,and the inter-group similarity evaluations were performed for the samples of different batches respective-ly,and the results showed that the angle cosine method could effectively detect the quality fluctuation of different batches of cigarette samples was examined.The Xbar-R control chart was applied to evaluate the quality variation level of cigarette products,and the results showed that the similarity of different batches of samples of five kinds of cigarettes was statistically controlled,and the similarity between batches of the prod-ucts was higher and the quality stability was better,which achieved effective monitoring of the quality stability of cigarette samples of different batches.[Conclusion]The volatile components of cigarette samples can be detected and analyzed rapidly and accurately by HS-GC-IMS,and the quality stability of cigarette products can be effectively assessed by combining the similarity evaluation and Xbar-R control chart.关键词
卷烟/顶空-气相色谱-离子迁移谱/指纹图谱/质量稳定性Key words
Cigarette/Headspace-gas chromatography-ion mobility spectrometry(HS-GC-IMS)/Fingerprinting/Quality stability分类
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张亮,刘显军,孙海峰,吕乔,苏凯,方程,杨鹏飞,吴薇,尚紫博..基于HS-GC-IMS技术评价卷烟的质量稳定性[J].安徽农业科学,2025,53(3):171-176,6.基金项目
中国烟草总公司重大科技项目[110202201053(SJ-03)] （SJ-03）
中国烟草实业发展中心科技项目(ZYSYQ-2022-17). （ZYSYQ-2022-17）
