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超声辅助氯化胆碱基低共熔溶剂提取银杏叶中多酚

于浩然 张径豪 牛静 毕胜胜 王锐

云南民族大学学报(自然科学版)2025,Vol.34Issue(1):13-19,7.
云南民族大学学报(自然科学版)2025,Vol.34Issue(1):13-19,7.DOI:10.3969/j.issn.1672-8513.2025.01.002

超声辅助氯化胆碱基低共熔溶剂提取银杏叶中多酚

Ultrasound-assisted extraction of polyphenols from Ginkgo biloba leaves using choline chloride-based deep eutectic solvent

于浩然 1张径豪 1牛静 2毕胜胜 1王锐3

作者信息

  • 1. 云南民族大学 化学与环境学院,云南 昆明 650500
  • 2. 浙江华友钴业股份有限公司,浙江 衢州 324000
  • 3. 云南民族大学 化学与环境学院,云南 昆明 650500||生物基材料绿色制备技术国家地方联合工程研究中心,云南 昆明 650500
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摘要

Abstract

In this study,the effect of deep eutectic solvents-based ultrasound-assisted extraction(DES-UAE)on the extraction of polyphenols from Ginkgo biloba leaves was investigated.Among seven prepared DES,choline chloride-DL-lactic acid was considered as a good candidate for polyphenols extraction due to its superior extrac-tion performance.Subsequently,the response surface methodology was used to explore the effect of process param-eters on the extraction rate,with the polyphenol extraction amount as the response value,and its process conditions were continuously optimized according to the extraction effect.The results showed that under the conditions of 40 kHz frequency ultrasound,the molar ratio of choline chloride:DL-lactic acid was 1∶3,the water volume frac-tion in DES was 32.32%,the extraction time was 50.5 min,and the liquid-solid ratio was 27.30 mL/g,13.73%of polyphenols were extracted from ginkgo leaves.This study provides a new idea for the extraction of polyphenolic compounds from Ginkgo biloba leaves,which reflects the advantages of DES in the extraction of polyphenolic com-pounds.

关键词

银杏叶多酚/低共熔溶剂/福林-酚比色法/超声提取/响应面法/绿色提取

Key words

Ginkgo biloba polyphenols/deep eutectic solvents/Folin-Ciocalteu colorimetry/ultrasonic extrac-tion/response surface method/green extraction

分类

轻工纺织

引用本文复制引用

于浩然,张径豪,牛静,毕胜胜,王锐..超声辅助氯化胆碱基低共熔溶剂提取银杏叶中多酚[J].云南民族大学学报(自然科学版),2025,34(1):13-19,7.

基金项目

国家自然科学基金(21862023). (21862023)

云南民族大学学报(自然科学版)

1672-8513

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