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强化固溶对Al-Mg-Si-Sn合金时效行为的影响

柳旭 刘春辉 马培培 湛利华 尹焯炀

中南大学学报(自然科学版)2025,Vol.56Issue(1):55-67,13.
中南大学学报(自然科学版)2025,Vol.56Issue(1):55-67,13.DOI:10.11817/j.issn.1672-7207.2025.01.006

强化固溶对Al-Mg-Si-Sn合金时效行为的影响

Effect of enhanced solid solution treatment on aging behavior of Al-Mg-Si-Sn alloy

柳旭 1刘春辉 2马培培 3湛利华 2尹焯炀1

作者信息

  • 1. 中南大学轻合金研究院,湖南 长沙,410083
  • 2. 中南大学轻合金研究院,湖南 长沙,410083||中南大学极端服役性能精准制造全国重点实验室,湖南 长沙,410083
  • 3. 中南大学高等研究中心,湖南 长沙,410083
  • 折叠

摘要

Abstract

The effect of solid solution temperature on the age-hardening behavior and microstructure of Al-Mg-Si-Sn alloy was investigated using Vickers microhardness tester and transmission electron microscopy(TEM).The results show that increasing the solid solution treatment(ST)temperature from 560℃to 590℃(enhanced solid solution temperature)significantly retards the natural aging(NA)of Al-Mg-Si-Sn alloy.After solid solution treatment and quenching,the time to peak hardness of natural aging is delayed from 3 d to 13 d.However,enhanced solid solution treatment does not significantly change the size of the precipitates of the peak aging state and the peak hardness of the artificially aged(AA)samples;the Sn-vacancy complex with a vacancy/Sn ratio greater than 1 is more stable,indicating that the enhanced solid solution treatment promotes the binding of Sn element to the vacancies through the simultaneous increase in the concentration of vacancies and the solubility of Sn,and thus retards the formation of natural aging clusters;the strengthening precipitates in artificial aging state are mainly β"/β'composite precipitates formed by heterogeneous nucleation on Sn-containing clusters;since the enhanced solid solution treatment can only slightly increase the solubility of Sn,its effect on the peak aging precipitation is very small;the different mechanisms of the Sn element lead to the different effects of enhanced solid solution treatment on natural aging and artificial aging.

关键词

Al-Mg-Si合金/固溶处理/Sn元素/自然时效/时效析出

Key words

Al-Mg-Si alloy/solid solution treatment/Sn element/natural aging/aging precipitation

分类

矿业与冶金

引用本文复制引用

柳旭,刘春辉,马培培,湛利华,尹焯炀..强化固溶对Al-Mg-Si-Sn合金时效行为的影响[J].中南大学学报(自然科学版),2025,56(1):55-67,13.

基金项目

国家自然科学基金资助项目(52305441,U2032117)(Projects(52305441,U2032117)supported by the National Natural Science Foundation of China) (52305441,U2032117)

中南大学学报(自然科学版)

OA北大核心

1672-7207

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