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基于ICP-MS测定聚丙烯腈纤维的铋含量

程羽君 濮杨 宗祥 吴建江 黄陈蓉 丁志峰

染整技术2025,Vol.47Issue(3):38-40,3.
染整技术2025,Vol.47Issue(3):38-40,3.

基于ICP-MS测定聚丙烯腈纤维的铋含量

Determination of bismuth content in polyacrylamide fiber based on ICP-MS

程羽君 1濮杨 1宗祥 2吴建江 1黄陈蓉 1丁志峰3

作者信息

  • 1. 绍兴市质量技术监督检测院国家纺织化学品质量检验检测中心(浙江),浙江 绍兴 312000
  • 2. 浙江竹子制药有限公司,浙江 绍兴 312300
  • 3. 绍兴市柯桥区生态环境分局,浙江 绍兴 312030
  • 折叠

摘要

Abstract

The detection limit of bismuth content detection method ICP-MS was 0.004 mg/kg,the limit of quantita-tion was 0.013 mg/kg,and the linear correlation coefficient R was 0.999 8.The standard recovery rate of the method was above 90%,and the detection results of the three quality control samples were all within the standard value range.Further verified by AFS detection,the RSD of the detection results of AFS and ICP-MS was<10%,fully verifying the accuracy of the detection method and the reliability of the equipment.The mass fraction of bismuth in 6 kinds of polyacrylonitrile fiber samples ranged from 0.08 to 3.31 mg/kg.

关键词

聚丙烯腈纤维/铋含量/准确性/ICP-MS

Key words

polyacrylonitrile fiber/bismuth content/accuracy/ICP-MS

分类

轻工纺织

引用本文复制引用

程羽君,濮杨,宗祥,吴建江,黄陈蓉,丁志峰..基于ICP-MS测定聚丙烯腈纤维的铋含量[J].染整技术,2025,47(3):38-40,3.

基金项目

浙江省市场监督管理局科研计划项目(ZC2021B089) (ZC2021B089)

染整技术

1005-9350

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