爆破器材2025，Vol.54Issue(2)：51-57,7.DOI:10.3969/j.issn.1001-8352.2025.02.007
一种用于固体推进剂样品无机组分含量测定的绿色预处理技术
A Green Pretreatment Technique for Determination of the Content of Inorganic Components in Solid Propellants
程秋霞 1薛小慧 1李佳佳 1张慧 1廉建彪1
作者信息
- 1. 山西北方兴安化学工业有限公司(山西 太原,030008)
- 折叠
摘要
Abstract
A green pretreatment method combining sealed infrared heating digestion technology with chemical ab-sorption of acid fume was used to wet decompose and pretreat solid propellant samples that require determination of inorga-nic component content,and absorb harmful acid fume generated by the reaction.The results show that during infrared hea-ting nitration,the content of combustion catalyst in the propellant meets the requirements by preheating for 5 min at 10%power of the electric furnace,heating for 30 min at 30%power,and then continuously heating for 40 min at 70%power.After preheating with an electric furnace at 10%power for 5 min,heating at 30%power for 30 min,and then continuously heating at 50%power for 60 min,the content of carbon black in the propellant meets the requirements.Zero emission of acid fume was achieved through two-stage absorption using alkaline solution with a mass fraction of 30%.The method is easy to operate,with high accuracy and precision,and can be used for sample pretreatment in the determination of inorga-nic component content in solid propellants.关键词
固体推进剂/酸烟/红外加热硝化/绿色预处理Key words
solid propellant/acid fume/infrared heating nitration/green pretreatment分类
化学工程引用本文复制引用
程秋霞,薛小慧,李佳佳,张慧,廉建彪..一种用于固体推进剂样品无机组分含量测定的绿色预处理技术[J].爆破器材,2025,54(2):51-57,7.
