信阳师范大学学报（自然科学版）2025，Vol.38Issue(2)：131-137,7.DOI:10.3969/j.issn.2097-583X.2025.02.002
溶胶-凝胶法与固相法制备BCZT陶瓷的结构与电学性能探究
Study on the structure and electrical properties of BCZT ceramics prepared by sol-gel method and solid phase method
摘要
Abstract
Ba0.85Ca0.15Zr0.1Ti0.9O3(BCZT)powder was prepared by a modified sol-gel method and traditional solid phase method,respectively.BCZT ceramics were prepared by a solid state reaction process at different sintering temperatures.The reaction process and structure of sol-gel powder were tested by X-ray diffraction,FT-IR spectrometer and thermal analyzer.The sintering process of ceramic was investigated by a high temperature image sintering instrument.The results showed that the best calcination temperature of BCZT powder prepared by sol-gel method was 900 ℃,the best sintering temperature of ceramic was 1400 ℃;While the best sintering temperature of ceramic prepared by solid phase method was 1500 ℃.The electrical property analysis showed that the relative permittivity and the remnant polarization of ceramics prepared by sol-gel method were 11 082.5 and 9.80 μC/cm2,respectively.The electrical properties of BCZT ceramics prepared by sol-gel process were greatly improved compared with those prepared by solid phase method.关键词
Ba0.85Ca0.15Zr0.1Ti0.9O3陶瓷/溶胶-凝胶法/固相法/物相结构/电学性能Key words
Ba0.85Ca0.15Zr0.1Ti0.9O3 ceramics/modified sol-gel method/solid phase method/phase structure/electrical properties分类
动力与电气工程引用本文复制引用
田永尚,马明扬,邵梦菲,陈玉芊,胡雄杰,刘鹏..溶胶-凝胶法与固相法制备BCZT陶瓷的结构与电学性能探究[J].信阳师范大学学报（自然科学版）,2025,38(2):131-137,7.基金项目
国家自然科学基金项目(51902279) （51902279）
河南省高等学校青年骨干教师培养计划(2021-GGJS-097) （2021-GGJS-097）
河南省重点研发与推广专项(科技攻关)(242102230158) （科技攻关）
信阳师范大学研究生科研创新基金项目(2024KYJJ072) （2024KYJJ072）
