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电感耦合等离子体发射光谱法测定丁辛醇废水中钠的不确定度评估

于雪 孙红珍 贲旭东 于海波 郑凌 宋权威

油气田环境保护2025,Vol.35Issue(2):49-54,6.
油气田环境保护2025,Vol.35Issue(2):49-54,6.DOI:10.3969/j.issn.1005-3158.2025.02.009

电感耦合等离子体发射光谱法测定丁辛醇废水中钠的不确定度评估

Uncertainty Assessment of Sodium Determination in Butanol-Octanol Wastewater by Inductively Coupled Plasma Emission Spectrometry

于雪 1孙红珍 1贲旭东 1于海波 1郑凌 1宋权威2

作者信息

  • 1. 中国石油天然气股份有限公司吉林石化分公司研究院
  • 2. 中国石油集团安全环保技术研究院有限公司
  • 折叠

摘要

Abstract

Inductively Coupled Plasma(ICP)emission spectrometry was used to determine the sodium(Na)content in butanol-octanol wastewater.The measurement uncertainty was calculated to objectively assess the accuracy of the test results and identify key points for improving method precision and accuracy.The results showed that the Na content in the butanol-octanol wastewater sample was(0.59±0.08)%(k=2),with a correlation coefficient of 0.999 8 for the calibration curve.The relative standard deviation(RSD)of the test results was 0.88%,which matched the sodium content determination results obtained by atomic absorption spectrometry for the same sample.This indicates that the method exhibits good precision and accuracy.

关键词

ICP发射光谱法/丁辛醇废水//测量不确定度

Key words

inductively coupled plasma emission spectrometry/butanol wastewater/sodium/measurement uncertainty

分类

石油、天然气工程

引用本文复制引用

于雪,孙红珍,贲旭东,于海波,郑凌,宋权威..电感耦合等离子体发射光谱法测定丁辛醇废水中钠的不确定度评估[J].油气田环境保护,2025,35(2):49-54,6.

基金项目

中国石油天然气集团有限公司科学研究与技术开发项目(2022DJ6906). (2022DJ6906)

油气田环境保护

1005-3158

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